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Fe(ClO4)3·H2O-Catalyzed Ritter Reaction: A Convenient Synthesis of Amides from Esters and Nitriles
Synlett ( IF 1.7 ) Pub Date : 2018-09-26 , DOI: 10.1055/s-0037-1610658 Min Ji 1 , Chengliang Feng 2 , Bin Yan 2 , Guibo Yin 2 , Junqing Chen 1
Synlett ( IF 1.7 ) Pub Date : 2018-09-26 , DOI: 10.1055/s-0037-1610658 Min Ji 1 , Chengliang Feng 2 , Bin Yan 2 , Guibo Yin 2 , Junqing Chen 1
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An efficient and inexpensive synthesis of N-substituted amides from the Ritter reaction of nitriles with esters catalyzed by Fe(ClO4)3·H2O is described. Fe(ClO4)3·H2O is an economically efficient catalyst for the Ritter reaction under solvent-free conditions. Reactions of a range of esters (benzyl, sec-alkyl, and tert-butyl esters) with nitriles (primary, secondary, tertiary, and aryl nitriles) were performed to provide the corresponding amides in high to excellent yields.
中文翻译：
Fe(ClO4)3·H2O-催化的里特反应：从酯和腈中方便地合成酰胺
描述了通过 Fe(ClO4)3·H2O 催化的腈与酯的 Ritter 反应高效且廉价地合成 N-取代酰胺。Fe(ClO4)3·H2O 是一种在无溶剂条件下进行 Ritter 反应的经济高效的催化剂。进行一系列酯（苄基、仲烷基和叔丁基酯）与腈（伯腈、仲腈、叔腈和芳基腈）的反应，以高产率至极好的产率提供相应的酰胺。
更新日期：2018-09-26
中文翻译：
Fe(ClO4)3·H2O-催化的里特反应：从酯和腈中方便地合成酰胺
描述了通过 Fe(ClO4)3·H2O 催化的腈与酯的 Ritter 反应高效且廉价地合成 N-取代酰胺。Fe(ClO4)3·H2O 是一种在无溶剂条件下进行 Ritter 反应的经济高效的催化剂。进行一系列酯（苄基、仲烷基和叔丁基酯）与腈（伯腈、仲腈、叔腈和芳基腈）的反应，以高产率至极好的产率提供相应的酰胺。
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