Dehydroxymethyl Bromination of Alkoxybenzyl Alcohols by Using a Hypervalent Iodine Reagent and Lithium Bromide,Synlett

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Dehydroxymethyl Bromination of Alkoxybenzyl Alcohols by Using a Hypervalent Iodine Reagent and Lithium Bromide
Synlett ( IF 1.7 ) Pub Date : 2018-09-26 , DOI: 10.1055/s-0037-1610980
Tomohiro Maegawa ₁ , Ayako Shibata ₁ , Sara Kitamoto ₁ , Kazuma Fujimura ₁ , Yuuka Hirose ₁ , Hiromi Hamamoto ₂ , Akira Nakamura _{1,

3} , Yasuyoshi Miki _{1,

3}

Affiliation

We describe the dehydroxymethylbromination of alkoxybenzyl alcohol by using a hypervalent iodine reagent and lithium bromide in F3CCH2OH at room temperature. Selective monobromination or dibromination was possible by adjusting the molar ratios of hypervalent iodine reagent and lithium bromide.

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