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A facile and novel route for the direct synthesis superparamagnetic ordered mesoporous carbon
Materials Letters ( IF 2.7 ) Pub Date : 2019-01-01 , DOI: 10.1016/j.matlet.2018.09.116
Xin Fu , Shaomin Liu , Dongliang Zhu , Yingbo Xu , Xiangyang Yan

Abstract In this paper, a novel soft-templating coupled with one-pot hydrothermal method has been developed to prepare magnetic ordered mesoporous carbon (Fe3O4-OMC) by using hexamine and resorcinol as the carbon source and triblock copolymer F127 as a template. Prepared Fe3O4-OMC possesses a large number of long and ordered mesoporous pore structures, the Fe3O4 nanoparticles were well embedded in the mesoporous carbon walls, and has a strong magnetization value of 39 emu g−1 and a narrow mesopore size distribution that peaked at 3.8 nm. The ordered channel of the Fe3O4-OMC is highly influenced by the quantity of Fe3O4 nanoparticles, hydrothermal reaction time and carbonization temperature.

中文翻译:

一种直接合成超顺磁性有序介孔碳的简便新途径

摘要 本文以六胺和间苯二酚为碳源,三嵌段共聚物F127为模板,开发了一种新型的软模板结合一锅水热法制备磁性有序介孔碳(Fe3O4-OMC)。制备的 Fe3O4-OMC 具有大量长而有序的介孔结构,Fe3O4 纳米粒子很好地嵌入介孔碳壁中,具有 39 emu g-1 的强磁化值和狭窄的介孔尺寸分布,峰值为 3.8纳米。Fe3O4-OMC 的有序通道受 Fe3O4 纳米粒子的数量、水热反应时间和碳化温度的影响很大。
更新日期:2019-01-01
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