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Fabrication process study of UCO composite ceramic microspheres with fructose as a carbon source by internal gelation and carbothermic reduction
Journal of Nuclear Materials ( IF 3.1 ) Pub Date : 2018-09-14 , DOI: 10.1016/j.jnucmat.2018.09.025
Xi Sun , Jingtao Ma , Xingyu Zhao , Shaochang Hao , Taowei Wang , Ziqiang Li , Changsheng Deng , Bing Liu

A preliminary study was carried out on preparation of UC-UO2 (UCO) composite ceramic microspheres using fructose as the carbon source by combining internal gelation and carbothermic reduction. The effects of the pH of precursor solution, washing and drying processes on the gel microspheres and sintering process on the UCO sintered microspheres were analyzed. The physical properties, composition, surface morphology and internal microstructure of the UCO ceramic microspheres were also studied. Dense and crack-free UCO ceramic microspheres with good sphericity, uniform composition distribution, and high crush strength were successfully fabricated.



中文翻译:

果糖为碳源的UCO复合陶瓷微球的内部凝胶化和碳热还原法制备工艺研究

以果糖为碳源,结合内部凝胶化和碳热还原法制备UC-UO 2(UCO)复合陶瓷微球进行了初步研究。分析了前体溶液的pH,洗涤和干燥过程对凝胶微球的影响以及烧结过程对UCO烧结微球的影响。还研究了UCO陶瓷微球的物理性质,组成,表面形貌和内部微观结构。成功制备了球形度好,组成分布均匀,抗碎强度高的致密无裂纹的UCO陶瓷微球。

更新日期:2018-09-14
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