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Extraction of anthocyanins from haskap berry pulp using supercritical carbon dioxide: Influence of co-solvent composition and pretreatment
LWT - Food Science and Technology ( IF 6.0 ) Pub Date : 2018-08-21 , DOI: 10.1016/j.lwt.2018.08.042
Guangling Jiao , Azadeh Kermanshahi pour

Extracts rich in anthocyanin compounds were obtained from haskap berry pulp paste using supercritical carbon dioxide (scCO2) and water as co-solvent. The extraction conditions including pressure, temperature, and amount of water were further optimized by Box-Behnken design. The highest total anthocyanins (TA) yield of 52.7% was achieved at 45 MPa, 65 °C, 5.4 g water to 3.2 g berry pulp paste, 15 min static and 20 min dynamic time. Different combinations of water and ethanol as co-solvent did not significantly affect the TA yield. Furthermore, similar anthocyanin extraction yields were obtained in the case of the pulp paste and rehydrated freeze-dried berry pulp powder, which indicates that freeze drying pretreatment is not required prior to scCO2 extraction. Compared with conventional extraction, the use of scCO2 and water as co-solvent offered higher anthocyanin extraction efficiency (52.7% versus 38.3%) with improved antioxidant activity (89.8% versus 72.2%).



中文翻译:

使用超临界二氧化碳从哈斯卡普果肉中提取花色苷:共溶剂组成和预处理的影响

使用超临界二氧化碳(scCO 2)和水作为助溶剂,从Haskap浆果浆糊中获得了富含花色苷化合物的提取物。通过Box-Behnken设计进一步优化了萃取条件,包括压力,温度和水量。在45 MPa,65°C,5.4克水至3.2克浆果果肉糊,15分钟静态和20分钟动态时间的条件下,最高总花色苷(TA)产率为52.7%。水和乙醇作为助溶剂的不同组合不会显着影响TA的收率。此外,在果肉糊和再水合的冷冻干燥的浆果果肉粉的情况下,获得了相似的花色苷提取率,这表明在scCO 2之前不需要进行冷冻干燥预处理。萃取。与常规提取相比,使用scCO 2和水作为共溶剂可提供更高的花色苷提取效率(52.7%对38.3%)和更高的抗氧化活性(89.8%对72.2%)。

更新日期:2018-08-21
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