Organocatalytic Cyclopropanation of (E)-Dec-2-enal: Synthesis, Spectral Analysis and Mechanistic Understanding,Journal of Chemical Education

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Organocatalytic Cyclopropanation of (E)-Dec-2-enal: Synthesis, Spectral Analysis and Mechanistic Understanding
Journal of Chemical Education ( IF 2.5 ) Pub Date : 2018-08-09 00:00:00 , DOI: 10.1021/acs.jchemed.7b00566
Marta Meazza ₁ , Agnieszka Kowalczuk ₁ , Sarah Watkins ₁ , Simon Holland ₁ , Thomas A. Logothetis ₁ , Ramon Rios ₁

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An undergraduate experiment combining synthesis, NMR analysis and mechanistic understanding is reported. The students perform an organocatalyzed cyclopropanation reaction of (E)-dec-2-enal and are then required to determine the diastereoselectivity and assign the relative configuration of each product using NMR spectroscopy.

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