Synthesis of self-assembled mesoporous 3D In2O3 hierarchical micro flowers composed of nanosheets and their electrochemical properties†,RSC Advances

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Synthesis of self-assembled mesoporous 3D In2O3 hierarchical micro flowers composed of nanosheets and their electrochemical properties†
RSC Advances ( IF 3.9 ) Pub Date : 2018-07-18 00:00:00 , DOI: 10.1039/c8ra03573c
Balasubramaniam Arul Prakasam _{1,

2} , Manu Lahtinen ₃ , Anssi Peuronen ₃ , Govindhasamy Manikandan ₂ , Manickavachagam Muruganandham ₁ , Mika Sillanpää _{1,

4}

Affiliation

This report describes the methodology for the fabrication of mesoporous In₂O₃ microflowers by hydrothermal and calcination procedures in which In(OH)₃/In₂S₃ acts as an intermediate. Both In₂O₃ and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray spectrophotometry, transmission electron microscopy and powder X-ray diffraction. BET surface area, pore size and pore volume analyses were also carried out. Electron microscopy images clearly evidence the self-assembly of 2D nanosheets into the micro flower structure. The mechanism of self-assembly and calcination is reported. Electrochemical properties of the synthesized In₂O₃ micro flowers were studied.

中文翻译：

由纳米片组成的自组装介孔 3D In2O3 分级微花的合成及其电化学性能†

本报告描述了通过水热法和煅烧法制备介孔 In ₂ O ₃微花的方法，其中 In(OH) ₃ /In ₂ S ₃作为中间体。用扫描电子显微镜、能量色散X射线分光光度法、透射电子显微镜和粉末X射线衍射分析了In ₂ O ₃及其前体。还进行了 BET 表面积、孔径和孔体积分析。电子显微镜图像清楚地证明了二维纳米片自组装成微花结构。报道了自组装和煅烧的机理。合成In的电化学性质_研究了2 O₃微花。

更新日期：2018-07-18

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