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Synthesis of self-assembled mesoporous 3D In2O3 hierarchical micro flowers composed of nanosheets and their electrochemical properties†
RSC Advances ( IF 3.9 ) Pub Date : 2018-07-18 00:00:00 , DOI: 10.1039/c8ra03573c
Balasubramaniam Arul Prakasam 1, 2 , Manu Lahtinen 3 , Anssi Peuronen 3 , Govindhasamy Manikandan 2 , Manickavachagam Muruganandham 1 , Mika Sillanpää 1, 4
Affiliation  

This report describes the methodology for the fabrication of mesoporous In2O3 microflowers by hydrothermal and calcination procedures in which In(OH)3/In2S3 acts as an intermediate. Both In2O3 and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray spectrophotometry, transmission electron microscopy and powder X-ray diffraction. BET surface area, pore size and pore volume analyses were also carried out. Electron microscopy images clearly evidence the self-assembly of 2D nanosheets into the micro flower structure. The mechanism of self-assembly and calcination is reported. Electrochemical properties of the synthesized In2O3 micro flowers were studied.

中文翻译:

由纳米片组成的自组装介孔 3D In2O3 分级微花的合成及其电化学性能†

本报告描述了通过水热法和煅烧法制备介孔 In 2 O 3微花的方法,其中 In(OH) 3 /In 2 S 3作为中间体。用扫描电子显微镜、能量色散X射线分光光度法、透射电子显微镜和粉末X射线衍射分析了In 2 O 3及其前体。还进行了 BET 表面积、孔径和孔体积分析。电子显微镜图像清楚地证明了二维纳米片自组装成微花结构。报道了自组装和煅烧的机理。合成In的电化学性质研究了2 O 3微花。
更新日期:2018-07-18
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