This work revises the essentials of electrocatalytic electrochemical measurement done in alkaline electrolytes. The hydrogen oxidation reaction (HOR) and the oxygen reduction reaction (ORR) were considered as a baseline to understand some key critical factors in a half-cell system. The material considered herein was essentially the carbon supported platinum nanoparticles as benchmark material. The main electrochemical techniques considered were cyclic voltammetry (CV) and the rotating disk electrode (RDE). The critical factors considered were the electrochemical cell vessel, reference electrode, nature of the cation in the alkaline electrolyte, and ohmic drop correction.

中文翻译：

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碱性电化学测量中HOR和ORR的实验方案

这项工作修改了在碱性电解质中进行电催化电化学测量的要点。氢氧化反应（HOR）和氧还原反应（ORR）被认为是了解半电池系统中一些关键关键因素的基线。本文考虑的材料基本上是作为基准材料的碳负载的铂纳米颗粒。所考虑的主要电化学技术是循环伏安法（CV）和旋转圆盘电极（RDE）。考虑的关键因素是电化学电池容器，参比电极，碱性电解质中阳离子的性质以及欧姆滴校正。