Towards a sustainable synthesis of amides: chemoselective palladium-catalysed aminocarbonylation of aryl iodides in deep eutectic solvents†,Chemical Communications

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Towards a sustainable synthesis of amides: chemoselective palladium-catalysed aminocarbonylation of aryl iodides in deep eutectic solvents†
Chemical Communications ( IF 4.3 ) Pub Date : 2018-06-25 00:00:00 , DOI: 10.1039/c8cc03858a
Francesco Messa _{1,

2,

3,

4} , Serena Perrone _{1,

2,

3,

4} , Martina Capua _{1,

2,

3,

4} , Francesco Tolomeo _{1,

2,

3,

4} , Luigino Troisi _{1,

2,

3,

4} , Vito Capriati _{4,

5,

6,

7,

8} , Antonio Salomone _{1,

2,

3,

4}

Affiliation

A palladium-catalysed aminocarbonylation of (hetero)aryl iodides has, for the first time, been accomplished in deep eutectic solvents as environmentally benign and recyclable media, under mild conditions. The reactions proceeded with a good substrate scope, and a variety of amides have been synthesized in yields up to 98%.

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