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Fabrication and characterization of carbon fiber reinforced SiC ceramic matrix composites based on 3D printing technology
Journal of the European Ceramic Society ( IF 5.8 ) Pub Date : 2018-06-15 , DOI: 10.1016/j.jeurceramsoc.2018.06.022
Wei Zhu , Hua Fu , Zhongfeng Xu , Rongzhen Liu , Ping Jiang , Xinyu Shao , Yusheng Shi , Chunze Yan

A novel method has been developed to fabricate carbon fiber reinforced SiC (Cf/SiC) composites by combining 3D printing and liquid silicon infiltration process. Green parts are firstly fabricated through 3D printing from a starting phenolic resin coated carbon fiber composite powder; then the green parts are subjected to vacuum resin infiltration and pyrolysis successively to generate carbon fiber/carbon (Cf/C) preforms; finally, the Cf/C preforms are infiltrated with liquid silicon to obtain Cf/SiC composites. The 3D printing processing parameters show significant effects on the physical properties of the green parts and also the resultant Cf/C preforms, consequently greatly affecting the microstructures and mechanical performances of the final Cf/SiC composites. The overall linear shrinkage of the Cf/SiC composites is less than 3%, and the maximum density, flexural strength and fracture toughness are 2.83 ± 0.03 g/cm3, 249 ± 17.0 MPa and 3.48 ± 0.24 MPa m1/2, respectively. It demonstrates the capability of making near net-shape Cf/SiC composite parts with complex structures.



中文翻译:

基于3D打印技术的碳纤维增强SiC陶瓷基复合材料的制备与表征

通过结合3D打印和液态硅渗透工艺,开发了一种新颖的方法来制造碳纤维增强SiC(C f / SiC)复合材料。首先通过3D打印从原始的酚醛树脂涂覆的碳纤维复合粉末中制造出绿色零件;然后将未加工的零件依次进行真空树脂渗透和热解,以生成碳纤维/碳(C f / C)预成型坯。最后,用液态硅渗透C f / C预成型坯以获得C f / SiC复合材料。3D打印处理参数对生坯的物理性能以及最终的C f均显示出显着影响/ C预成型坯,因此极大地影响了最终C f / SiC复合材料的微观结构和力学性能。的C的整体线性收缩˚F / SiC复合材料是小于3%,并且最大密度,弯曲强度和断裂韧性是2.83±0.03克/厘米3,249±17.0兆帕和3.48±0.24兆帕米1/2,分别。它展示了制造具有复杂结构的近净形C f / SiC复合零件的能力。

更新日期:2018-06-15
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