In this research, tungsten disulfide (WS₂) nanosheets as sonocatalyst were synthesized through a sonochemical route. Characterization of as-synthesized sonocatalyst was carried out by X-ray diffraction (XRD), scanning electron microscopy (SEM), electron dispersive X-ray spectroscopy (EDX), Dot-mapping, high resolution transmission electron microscopy (HRTEM), Brunauer-Emmett-Teller (BET), Fourier transform infrared spectroscopy (FTIR), and ultraviolet-visible diffuse reflectance spectroscopy (UV-vis DRS) analysis. WS₂ nanosheets were evaluated for their sonocatalytic performance in order to remove basic violet 10 (BV10) under ultrasonic irradiation. The removal efficiency was maximized (94.01%) via the use of 1 g L^-1 catalyst and 10 mg L^-1 BV10 at pH = 4.5 and an ultrasonic power of 400 W within a reaction time of 150 min. In addition to BV10, the sonocatalytic elimination for a number of organic dyes viz. direct blue 71, acid blue 92, methylene blue, basic orange 2 and basic red 46 was examined to demonstrate the performance of WS₂ nanosheets under the ultrasonic irradiation. The experimentation of trapping was conducted using edetate disodium (EDTA-2Na), tert-butyl alcohol (t-BuOH), and benzoquinone (BQ). According to the results, all radicals participated in the sonocatalytic activity. ^•OH played a more prominent role than h⁺ and $O_2^{-\bullet }$in the process of BV10 separation. Following five repetitive runs, the nanocomposites revealed a reusability of circa 18% drop in the elimination efficiency. The main removal intermediates were recognized by GC-MS technique.

在这项研究中，通过声化学途径合成了二硫化钨（WS ₂）纳米片作为声催化剂。通过X射线衍射（XRD），扫描电子显微镜（SEM），电子色散X射线光谱（EDX），点映射，高分辨率透射电子显微镜（HRTEM），Brunauer- Emmett-Teller（BET），傅立叶变换红外光谱（FTIR）和紫外可见漫反射光谱（UV-vis DRS）分析。评估WS ₂纳米片的声催化性能，以便在超声辐射下去除碱性紫10（BV10）。通过使用1 g L ^-1 催化剂和10 mg L ^-1可以最大程度地提高去除效率（94.01％） 在150分钟的反应时间内，pH = 4.5的BV10和400 W的超声功率。除BV10外，还对多种有机染料进行了声催化消除。检查了直接蓝71，酸性蓝92，亚甲基蓝，碱性橙2和碱性红46，以证明WS ₂纳米片在超声辐射下的性能。使用乙二胺四乙酸二钠（EDTA-2Na），叔丁醇（t - BuOH）和苯醌（BQ）进行捕获实验。根据结果​​，所有自由基都参与了声催化活性。^• OH的作用比h ⁺和${Ø}_{\mathrm{2个}}^{--\bullet }$在BV10分离过程中。经过五次重复运行，纳米复合材料的消除效率降低了约18％。主要去除中间体已通过GC-MS技术进行了识别。