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Alkoxylation Followed by Iodination of Oxindole with Alcohols Mediated by Hypervalent Iodine Reagent in the Presence of Iodine
European Journal of Organic Chemistry ( IF 2.5 ) Pub Date : 2018-08-17 , DOI: 10.1002/ejoc.201800723
Rajendraprasad Kotagiri 1, 2 , Ramesh Adepu 3
Affiliation  

Iodoalkoxylation of oxindole with alcohols was achieved by using a hypervalent iodine species in combination with iodine under metal‐free conditions. This method is useful for the synthesis of 3‐alkoxy oxindole, 5‐iodo‐3‐alkoxy oxindole and 5‐iodo‐3,3‐dialkoxy oxindole by sequentially in moderate to good yields.
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中文翻译:

在碘存在的情况下进行烷氧基化,然后用高价碘试剂介导的醇对羟吲哚进行碘化

在无金属条件下,结合使用高价碘和碘,可以实现羟吲哚与醇的碘烷氧基化。该方法可用于以中等到良好的收率顺序合成3-烷氧基羟吲哚,5-碘-3-3-烷氧基羟吲哚和5-碘-3-3,3-二烷氧基羟吲哚。
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更新日期:2018-08-17
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