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Two quite different primary Mn-rich phases in Al-Si-Cu-Mn heat-resistant alloy and its effect to mechanical properties
Materials Science and Engineering: A ( IF 6.1 ) Pub Date : 2018-05-26 , DOI: 10.1016/j.msea.2018.05.100
Guangjing Li , Hengcheng Liao , Aiqun Xu

Two quite different primary Mn-rich phases were observed by optical microscope and scanning electron microscope in the surface and central parts of Al-12 wt%Si-4 wt%Cu-2 wt%Mn heat-resistant alloy casting. Deep-etching observation reveals that one is as highly developed 3D-dendrites and the other is as simple 2D-laths. The results of SEM-EDS show the constituents of these two Mn-rich phases are quite different too. The results of TEM-EDS verify it further. By selected area electron diffraction pattern, the lath-shaped Mn-rich phase is identified as: Al13Mn4Si8, simple tetragonal, a = b = 1.240 nm, c = 0.489 nm. The tension test indicates the contribution to strength from dendritic Al15Mn3Si2 phase is larger than Al13Mn4Si8 phase whether at room temperature or at high temperature. The reason for it is thought to be tied with the much larger difference in elastic modulus of Al13Mn4Si8 phase with aluminum matrix than that of Al15Mn3Si2.



中文翻译:

Al-Si-Cu-Mn耐热合金中两个完全不同的富锰初生相及其对机械性能的影响

通过光学显微镜和扫描电子显微镜在Al-12 wt%Si-4 wt%Cu-2 wt%Mn耐热合金铸件的表面和中央部分观察到两个完全不同的富锰主相。深蚀刻观察发现,一个像高度发达的3D树枝状晶体,另一个像简单的2D板条。SEM-EDS的结果表明,这两个富锰相的成分也完全不同。TEM-EDS的结果进一步证明了这一点。通过选择的区域电子衍射图,板条状富锰相被确定为:Al 13 Mn 4 Si 8,简单四方,a = b = 1.240 nm,c = 0.489 nm。拉伸试验表明树枝状Al 15 Mn 3 Si 2对强度的贡献无论在室温还是在高温下,该相都大于Al 13 Mn 4 Si 8相。认为其原因与铝基质的Al 13 Mn 4 Si 8相的弹性模量比Al 15 Mn 3 Si 2的相差更大。

更新日期:2018-05-26
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