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Combining C-H functionalisation and flow photochemical heterocyclic metamorphosis (FP-HM) for the synthesis of benzo[1,3]oxazepines
Tetrahedron ( IF 2.1 ) Pub Date : 2018-05-24 , DOI: 10.1016/j.tet.2018.05.066
Jasraj S. Babra , Andrew T. Russell , Christopher D. Smith , Yuxiong Zhang

C-H Activation/functionalisation and Flow Photochemical Heterocyclic Metamorphosis (FP-HM) have been combined to synthesize a library of benzo [1,3]oxazepines, a rarely described heterocyclic family. This combined protocol allows a range of arylated products to be made from simple starting materials, and the cheap flow photochemical system has proven effective for rapid synthesis of gram-quantities of benzo [1,3]oxazepines.



中文翻译:

结合CH功能化和流式光化学杂环变态反应(FP-HM)合成苯并[1,3]氧氮杂pine

CH激活/功能化和流光化学杂环变态反应(FP-HM)已被组合以合成苯并[1,3]氮杂氮杂文库,这是一个鲜为人知的杂环家族。该组合方案允许使用简单的起始原料制备多种芳基化产品,并且廉价的流动光化学体系已被证明可有效地快速合成革兰氏量的苯并[1,3]氮杂ze庚因。

更新日期:2018-05-24
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