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Nanofibers of cellulose bagasse from Agave tequilana Weber var. azul by electrospinning: preparation and characterization
Carbohydrate Polymers ( IF 11.2 ) Pub Date : 2018-03-19 , DOI: 10.1016/j.carbpol.2018.03.058
Miguel Ángel Robles-García , Carmen Lizette Del-Toro-Sánchez , Enrique Márquez-Ríos , Arturo Barrera-Rodríguez , Jacobo Aguilar , José A. Aguilar , Francisco Javier Reynoso-Marín , I. Ceja , R. Dórame-Miranda , Francisco Rodríguez-Félix

In this study, cellulose of bagasse from Agave tequilana Weber var. azul was extracted to elaborate nanofibers by the electrospinning technique. Fiber characterization was performed using Transmission Electron Microscopy (TEM), x-ray, Fournier Transform-InfraRed (FT-IR) spectroscopy, and thermal analysis by Differential Scanning Calorimetry-Thermogravimetric Analysis (DSC-TGA). Different diameters (ranging from 54.57 ± 0.02 to 171 ± 0.01 nm) of nanofibers were obtained. Cellulose nanofibers were analyzed by means of x-ray diffraction, where we observed a total loss of crystallinity in comparison with the cellulose, while FT-IR spectroscopy revealed that the hemicellulose and lignin present in the agave bagasse were removed. Thermal analysis showed that nanofibers exhibit enhanced thermal properties, and the zeta potential value (-32.5 mV) demonstrated moderate stability in the sample. In conclusion, the nanofibers obtained provide other alternatives-of-use for this agro-industrial residue and could have potential in various industrial applications, among these encapsulation of bioactive compounds and reinforcing material, to mention a few.



中文翻译:

龙舌兰纤维的纤维素甘蔗渣的纳米纤维。静电纺丝azul:制备和表征

在这项研究中,来自龙舌兰龙舌兰酒Weber var的蔗渣纤维素。阿祖尔通过静电纺丝技术提取了纳米纤维,从而制成了纳米纤维。使用透射电子显微镜(TEM),x射线,傅立叶变换红外(FT-IR)光谱和差示扫描量热法-热重分析(DSC-TGA)进行热分析,进行纤维表征。获得了不同直径的纳米纤维(范围从54.57±0.02到171±0.01 nm)。通过X射线衍射分析了纤维素纳米纤维,与纤维素相比,我们观察到结晶度完全丧失,而FT-IR光谱显示龙舌兰蔗渣中存在的半纤维素和木质素被去除。热分析表明,纳米纤维表现出增强的热性能,并且ζ电势值(-32.5 mV)在样品中表现出中等的稳定性。综上所述,

更新日期:2018-03-20
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