A nanostructured cationic zinc nitrate complex with a formula of [ZnLNO₃]NO₃ (where L= (N²E,N^2'E)-N¹,N^1'-(ethane-1,2-diyl)bis(N²-((E)-3-phenylallylidene)ethane-1,2-diamine)) was prepared by sonochemical process and characterized by single crystal X-ray crystallography, scanning electron microscopy (SEM), FT-IR and NMR spectroscopy and X-ray powder diffraction (XPRD). The X-ray analysis demonstrates the formation of a cationic complex that metal center is five-coordinated by four nitrogen atom from Schiff base ligand and one oxygen atom from nitrate group. The crystal packing analysis demonstrates the essential role of the nitrate groups in the organization of supramolecular structure. The morphology and size of ultrasound-assisted synthesized zinc nitrate complex have been investigated using scanning electron microscopy (SEM) by changing parameters such as the concentration of initial reactants, the sonication power and reaction temperature. In addition the calcination of zinc nitrate complex in air atmosphere led to production of zinc oxide nanoparticles.

纳米结构化的阳离子硝酸锌配合物的式[ZnLNO ₃ ] NO ₃（其中L =（N ² E，N ^2' E）-N ¹，N ^1' - （乙烷-1,2-二基）双（N ^2个-（（E）-3-苯基亚烷基）乙烷-1,2-二胺））是通过声化学方法制备的，并通过单晶X射线晶体学，扫描电子显微镜（SEM），FT-IR和NMR光谱以及X-进行了表征。射线粉末衍射（XPRD）。X射线分析表明形成了一种阳离子络合物，该金属络合物由席夫碱配体的四个氮原子和硝酸盐基团的一个氧原子五配位。晶体堆积分析证明了硝酸根基团在超分子结构的组织中的重要作用。超声辅助合成硝酸锌配合物的形态和尺寸已通过扫描电子显微镜（SEM）通过改变初始反应物浓度，超声处理功率和反应温度等参数进行了研究。