YbVO₄ nanostructure and YbVO₄/CuWO₄ nanocomposites were successfully synthesized using sonochemical method, for the first time. In this disquisition, we tried to compare various parameters and reaction conditions on size, morphology, and uniformity of as-obtained samples. To reach optimum condition, some parameters including time, power, temperature, and solvent were investigated. The structural, morphological, optical, and magnetic properties of as-obtained products were characterized by some techniques such as FT-IR, XRD, EDS, SEM, TEM, UV-Vis, and VSM. Furthermore, due to occurrence of red shift in nonanocomposite, during the coupling of CuWO₄ into YbVO₄, photocatalytic and optical properties of final products were improved which lead to improve photo-destruction efficiency for methylene blue from 65% to 100%, during 120 min irradiation. The effect of the ultrasonic radiation on the photocatalytic behavior of YbVO₄/CuWO₄ shows that methylene blue pollutant destruction was about 100% with ultrasonic wave and 61% in the absence of ultrasonic radiation.

首次采用声化学方法成功合成了YbVO ₄纳米结构和YbVO ₄ / CuWO ₄纳米复合材料。在本次研究中，我们试图比较各种参数和反应条件对所获得样品的大小，形态和均匀性的影响。为了达到最佳条件，研究了一些参数，包括时间，功率，温度和溶剂。通过诸如FT-IR，XRD，EDS，SEM，TEM，UV-Vis和VSM等技术来表征所获得产品的结构，形态，光学和磁性。此外，由于在非纳米复合材料中发生红移，因此在CuWO ₄偶联到YbVO _4中，最终产物的光催化和光学性能得到改善，从而在120分钟的照射过程中，亚甲基蓝的光解效率从65％提高到100％。超声波辐射对YbVO ₄ / CuWO ₄的光催化行为的影响表明，在超声波作用下，亚甲基蓝污染物的破坏程度约为100％，在没有超声波辐射的情况下，破坏程度为61％。