Abstract The electrochemical oxidation of 2-nitroso-1-naphthol (2N1N) in the absence and presence of some arylsulfinic acids in aqueous buffer/ethanol (30/70 v/v) mixtures has been studied. We were able to determine the pH-dependence behavior of 2N1N on the one hand and the changes on the voltammetric response of 2N1N that are caused by arylsulfinic acids, on the other hand. In addition, some new sulfonamide derivatives have been synthesized from the reaction of 2N1N with arylsulfinic acids, via a very simple and green method.

中文翻译：

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磺胺合成的循环伏安辅助机械评价。N-(1-羟基萘-2-基)苯磺酰胺衍生物的简单绿色合成方法

摘要 研究了在缓冲液/乙醇 (30/70 v/v) 混合物中存在和存在某些芳基亚磺酸的情况下 2-亚硝基-1-萘酚 (2N1N) 的电化学氧化。我们能够一方面确定 2N1N 的 pH 依赖性行为，另一方面确定由芳基亚磺酸引起的 2N1N 伏安响应的变化。此外，通过一种非常简单和绿色的方法，通过 2N1N 与芳基亚磺酸的反应合成了一些新的磺酰胺衍生物。