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3D Micropatterned All-Flexible Microfluidic Platform for Microwave-Assisted Flow Organic Synthesis.
ChemPlusChem ( IF 3.0 ) Pub Date : 2018-01-01 , DOI: 10.1002/cplu.201700440
Deniz Hur 1, 2 , Mehmet G Say 2, 3 , Sibel E Diltemiz 1, 2 , Fatma Duman 1 , Arzu Ersöz 1, 2 , Rıdvan Say 1, 2
Affiliation  

A large-area, all-flexible, microwaveable polydimethoxysilane microfluidic reactor was fabricated by using a 3D printing system. The sacrificial microchannels were printed on polydimethoxysilane substrates by a direct ink writing method using water-soluble Pluronic F-127 ink and then encapsulated between polydimethoxysilane layers. The structure of micron-sized channels was analyzed by optical and electron microscopy techniques. The fabricated flexible microfluidic reactors were utilized for the acetylation of different amines under microwave irradiation to obtain acetamides in shorter reaction times and good yields by flow organic synthesis.

中文翻译:

用于微波辅助流动有机合成的3D微图案全柔性微流体平台。

通过使用3D打印系统制造了大面积,全柔性,可微波加热的聚二甲氧基硅烷微流体反应器。通过使用水溶性Pluronic F-127墨水的直接墨水书写方法,将牺牲微通道打印在聚二甲氧基硅烷基材上,然后封装在聚二甲氧基硅烷层之间。通过光学和电子显微镜技术分析了微米级通道的结构。所制备的柔性微流体反应器用于微波辐射下不同胺的乙酰化,以较短的反应时间和通过流动有机合成获得良好收率的乙酰胺。
更新日期:2018-01-15
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