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Effect of pH on the synthesis of In(OH)3 and In(OH)3:Ce3+/Dy3+ nanocrystals by a fast, mild microwave method
Journal of Solid State Chemistry ( IF 3.3 ) Pub Date : 2017-10-09 , DOI: 10.1016/j.jssc.2017.10.010
Yinyan Li , Ruoshan Lei , Shiqing Xu

Indium hydroxide nanocrystals were synthesized through a microwave reaction. It is a fast, simple and mild process to get the uniform and monodisperse In(OH)3 nanomaterials without the aid of any surfactants or templates. Size and morphology of the In(OH)3 nanomaterials could be controllably adjusted through the pH value of the reaction mixtures. The formation mechanisms of the nanostructures have been investigated on the basis of a series of SEM studies of the samples obtained at different reaction durations. Ce3+, Dy3+ or Ce3+/Dy3+ doped In(OH)3 were also synthesized by the microwave reaction and optical properties of these materials were evaluated.



中文翻译:

pH对快速温和微波法合成In(OH)3和In(OH)3:Ce 3+ / Dy 3+纳米晶体的影响

通过微波反应合成了氢氧化铟纳米晶体。在不借助任何表面活性剂或模板的情况下,获得均匀且单分散的In(OH)3纳米材料是一种快速,简单且温和的过程。In(OH)3纳米材料的大小和形态可以通过反应混合物的pH值来控制。基于在不同反应持续时间下获得的样品的一系列SEM研究,已经研究了纳米结构的形成机理。还通过微波反应合成了掺杂Ce 3+,Dy 3+或Ce 3+ / Dy 3+的In(OH)3,并评价了这些材料的光学性质。

更新日期:2017-12-14
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