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Antibacterial studies of novel Cu2WS4 ternary chalcogenide synthesized by hydrothermal process
Journal of Solid State Chemistry ( IF 3.3 ) Pub Date : 2017-11-03 , DOI: 10.1016/j.jssc.2017.11.005
Selvaraj Kannan , Perumal Vinitha , Kannusamy Mohanraj , Ganesan Sivakumar

This is the first report for the synthesis of L-cysteine mediated Cu2WS4 nanoparticles for different temperatures by an inexpensive and less pollutive hydrothermal method. The as-synthesized particles were characterized by XRD, FTIR, FESEM, UV–vis diffuse reflectance and PL spectra technique respectively. The phase purity and structural confirmation were studied by X-ray powder diffraction technique. It is observed that the synthesis temperature affecting the crystalline size. The optical analysis of the Cu2WS4 nanoparticles showed direct band gap in the range of 2.1–2.3 eV. The intensity of the PL emission spectra decreases with increase of reaction temperature. The antibacterial performance of Cu2WS4 nanoparticles were investigated by agar well diffusion method and the results confirm that the antibacterial activity of Cu2WS4 against Gram-positive (B. subtilis, M. luteus) and Gram-negative (E. coli, P. aeruginosa and K. pneumoniae) bacteria.



中文翻译:

水热法合成新型Cu 2 WS 4三元硫属元素的抗菌研究

这是通过廉价且污染少的水热法合成不同温度下L-半胱氨酸介导的Cu 2 WS 4纳米粒子的第一份报告。分别通过XRD,FTIR,FESEM,UV-vis漫反射和PL光谱技术对合成后的颗粒进行了表征。通过X射线粉末衍射技术研究了相纯度和结构确认。观察到合成温度影响晶体尺寸。Cu 2 WS 4纳米粒子的光学分析显示直接带隙在2.1–2.3范围内 eV。PL发射光谱的强度随着反应温度的升高而降低。通过琼脂井扩散法研究了Cu 2 WS 4纳米颗粒的抗菌性能,结果证实了Cu 2 WS 4对革兰氏阳性(枯草芽孢杆菌,黄曲霉)和革兰氏阴性菌(大肠杆菌)的抗菌活性。 ,铜绿假单胞菌和肺炎克雷伯菌)。

更新日期:2017-12-14
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