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TEM characterization on new 9% Cr advanced steels thermomechanical treated after tempering
Journal of Nuclear Materials ( IF 3.1 ) Pub Date : 2017-12-14 , DOI: 10.1016/j.jnucmat.2017.12.025
P. Fernández , J. Hoffmann , M. Rieth , M. Roldán , A. Gómez-Herrero

Phase transformation on new six reduced activation ferritic/martensitic steels (RAFMs) was investigated to provide the basis for the design and development of advanced steels to maintain adequate strength and creep resistance above 500 °C. The new alloys are designed to increase the amount of fine MX precipitates and reduce coarse M23C6 carbides through alloy composition refinement and the application of thermomechanical treatments. The microstructural investigations by TEM have shown M23C6, M2X, and MX precipitation after tempering at 700 °C/2h with low dislocation recovery, while at 825 °C/2h the martensite developed to subgrain formation and growth. At this stage, only M23C6 and MX were detected. Preliminary results demonstrate that it is feasible to produce fine MX strengthened particles dispersed in the matrix with further optimization of tempering treatments.



中文翻译:

回火后经过热机械处理的新型9%Cr高级钢的TEM表征

研究了六种新的还原活化铁素体/马氏体钢(RAFM)的相变,为高级钢的设计和开发提供了基础,以在500°C以上保持足够的强度和抗蠕变性。通过合金成分的细化和热机械处理的应用,这些新合金旨在增加细小的MX析出物的数量并减少粗大的M 23 C 6碳化物。TEM的显微组织研究表明,在700°C / 2h回火后,M 23 C 6,M 2 X和MX析出,位错回复率低,而在825°C / 2h时,马氏体发展为亚晶粒形成和生长。在这个阶段,只有M 23 C检测到6和MX。初步结果表明,通过进一步优化回火处理,可以生产出分散在基质中的细MX增强颗粒。

更新日期:2017-12-14
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