Intermetallic ternary Mo-nitrides are important functional materials due to their unique physical and chemical properties. However, the preparation of this class of materials is usually divided into two steps: the first step is the preparation of the ternary oxides, the second step is the nitridation of the ternary oxides. In this study, a facile procedure for synthesizing ternary Mo-nitrides has been reported. Co₃Mo₃N and Fe₃Mo₃N nanoparticles have been synthesized by a one step solid state reaction in a sealed autoclave at 750 °C. The structures and morphologies of the obtained products are derived from X-ray diffraction and electron microscopy. Furthermore, the oxidation resistances and magnetic properties of the obtained products have been investigated.

中文翻译：

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一步固相反应合成三元氮化物Co ₃ Mo ₃ N和Fe ₃ Mo ₃ N

金属间三元氮化物由于其独特的物理和化学性质而成为重要的功能材料。但是，这类材料的制备通常分为两个步骤：第一步是三元氧化物的制备，第二步是三元氧化物的氮化。在这项研究中，已经报道了一种简便的合成三元氮化钼的方法。Co ₃ Mo ₃ N和Fe ₃ Mo ₃通过在750°C的密闭高压釜中进行一步固态反应合成了N纳米颗粒。所得产物的结构和形态是由X射线衍射和电子显微镜得到的。此外，已经研究了所得产物的抗氧化性和磁性。