Current-use pesticides (CUPs) are the replacements of legacy organochlorine pesticides. The increasing use of CUPs has resulted in their occurrence in various environmental matrices including water, air, soil and sediment. The diversity in the physicochemical properties of CUPs and the complexity of the matrices pose challenges in the selection and optimization of laboratory methods for their measurement. This review provides a summary and comparison of different methods used in the sample extraction, extract cleanup, and instrumental analysis for the determination of CUPs in abiotic environmental matrices. About 150 papers are reviewed, most were published between 2015 and 2023. Solid phase extraction, pressurized liquid extraction, QuEChERS, GC-MS and LC-MS/MS are the major techniques adopted in most studies. Environmental friendliness, microscale, automation, and sensitivity are the developing trends of CUPs analysis. This review is useful for analytical method development and future research on CUPs in water, air, soil, and sediment.

中文翻译：

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非生物环境基质中当前使用农药的样品制备和分析趋势

当前使用的农药 (CUP) 是传统有机氯农药的替代品。CUP 的使用越来越多，导致它们出现在各种环境基质中，包括水、空气、土壤和沉积物。CUP 物理化学性质的多样性和基质的复杂性给实验室测量方法的选择和优化带来了挑战。本综述对用于测定非生物环境基质中 CUP 的样品提取、提取物净化和仪器分析中使用的不同方法进行了总结和比较。综述了约 150 篇论文，大多数发表于 2015 年至 2023 年之间。固相萃取、加压液体萃取、QuEChERS、GC-MS 和 LC-MS/MS 是大多数研究采用的主要技术。环境友好、微量化、自动化、灵敏化是CUP分析的发展趋势。本综述对于水、空气、土壤和沉积物中 CUP 的分析方法开发和未来研究非常有用。