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Convenient preparation of dichloromethyl alkyl ethers
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2017-10-26 , DOI: 10.1016/j.tetlet.2017.10.052
Yoshikazu Kimura , Takuya Warashina

Dichloromethyl alkyl ethers have been synthesized from alkyl formates (C1–C4) and oxalyl chloride in the presence of catalytic amount of N-methylformanilide. N,N-Dimethylformamide is not suitable for the reaction. The method has the advantages of simple experimental procedure, which is applicable to large scale synthesis, without use of harmful reagents.



中文翻译:

方便的二氯甲基烷基醚的制备

在催化量的N-甲基甲酰苯胺存在下,由烷基甲酸酯(C1-C4)和草酰氯合成了二氯甲基烷基醚。NN-二甲基甲酰胺不适合该反应。该方法具有实验过程简单,适用于大规模合成,无需使用有害试剂的优点。

更新日期:2017-10-26
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