当前位置: X-MOL 学术J. Org. Chem. › 论文详情
Our official English website, www.x-mol.net, welcomes your feedback! (Note: you will need to create a separate account there.)
Synthesis of Azobenzenes Using N-Chlorosuccinimide and 1,8-Diazabicyclo[5.4.0]undec-7-ene (DBU)
The Journal of Organic Chemistry ( IF 3.3 ) Pub Date : 2017-09-07 00:00:00 , DOI: 10.1021/acs.joc.7b01530
Alford Antoine John 1 , Qing Lin 1
Affiliation  

A convenient method for the synthesis of symmetrical azobenzenes is reported. This one-step procedure involves treatment of anilines with N-chlorosuccinimide (NCS) and organic base 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU). A wide range of commercially available substituted anilines readily participate in this reaction to produce the corresponding azobenzenes in moderate-to-excellent yields in minutes.

中文翻译:

N-氯代琥珀酰亚胺和1,8-二氮杂双环[5.4.0]十一碳-7-烯(DBU)合成偶氮苯

据报道,一种方便的合成对称的偶氮苯的方法。此一步步骤涉及用N-氯代琥珀酰亚胺(NCS)和有机碱1,8-二氮杂双环[5.4.0]十一碳-7-烯(DBU)处理苯胺。多种可商购的取代苯胺容易参与该反应,以在数分钟内以中等至优异的产率产生相应的偶氮苯。
更新日期:2017-09-07
down
wechat
bug