A Convenient, Mild, and Green Synthesis of NH-Sulfoximines in Flow Reactors,European Journal of Organic Chemistry

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A Convenient, Mild, and Green Synthesis of NH-Sulfoximines in Flow Reactors
European Journal of Organic Chemistry ( IF 2.5 ) Pub Date : 2017-09-05 07:35:51 , DOI: 10.1002/ejoc.201700850
Leonardo Degennaro ₁ , Arianna Tota ₁ , Sonia De Angelis ₁ , Michael Andresini ₁ , Cosimo Cardellicchio ₂ , Maria Annunziata Capozzi ₃ , Giuseppe Romanazzi ₄ , Renzo Luisi ₁

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We report herein the development of an efficient, convenient, and sustainable continuous-flow strategy for the direct, straightforward preparation of NH-sulfoximines starting either from sulfides or from sulfoxides. The flow process uses PhI(OAc)₂ as the oxidant and aqueous solutions of ammonia as the N source. The flow strategy was found to be more convenient than the conventional batch processing.

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