Neutralization of a Toluene Waste Stream Containing Thionyl Chloride,Organic Process Research & Development

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Neutralization of a Toluene Waste Stream Containing Thionyl Chloride
Organic Process Research & Development ( IF 3.1 ) Pub Date : 2017-08-17 00:00:00 , DOI: 10.1021/acs.oprd.7b00195
J. Robert Durrwachter ₁

Affiliation

Neutralization of thionyl chloride in toluene was found to be ineffective with water. A solution is to use an excess of a soluble reagent to consume the thionyl chloride. Butanol was shown to convert thionyl chloride to n-butyl sulfite and hydrogen chloride. An aqueous workup removes any residual hydrogen chloride.

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