Unprecedented Carbon Signal Enhancement in Liquid-State NMR Spectroscopy.,Angewandte Chemie International Edition

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Unprecedented Carbon Signal Enhancement in Liquid-State NMR Spectroscopy.
Angewandte Chemie International Edition ( IF 16.1 ) Pub Date : 2017-05-23 , DOI: 10.1002/anie.201702766
György Pintér ₁ , Harald Schwalbe ₁

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We shall overcome: As a result of efforts to overcome the sensitivity challenge of liquid-state NMR spectroscopy, a thousand-fold signal enhancement was achieved by dynamic nuclear polarization (DNP) for 13 C signals at high magnetic field (3.4 T) and room temperature, thereby exceeding the predicted limitations of high-field liquid-state in situ DNP.

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