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Synthesis and structural peculiarities of disodium 1,6-dioxoalka-2,4-diene-3,4-diolates

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Abstract

Three-component condensation of dialkyl oxalates with alkyl acetates and alkyl methyl ketones in the presence of bases afforded 1-alkoxy(or 1,6-dialkoxy)-1,6-dioxoalka-2,4-diene-3,4-diolates. The product structure was discussed on the basis of their IR, 1H NMR, and mass spectra.

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References

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Authors and Affiliations

  1. Institute for Cellular and Intracellular Symbiosis, Ural Branch, Russian Academy of Scuences, ul. Pionerskaya 11, Orenburg, 460000, Russia

    P. P. Mukovoz

  2. Orenburg State University, pr. Pobedy 13, Orenburg, 460018, Russia

    V. A. Andreeva & V. O. Koz’minykh

  3. Perm State Humanitarian Pedagogical University, Sibirskaya ul. 24, Perm, 614990, Russia

    V. O. Koz’minykh & E. N. Koz’minykh

  4. Yeltsin Ural Federal University, ul. Mira 32, Yekaterinburg, 620062, Russia

    O. S. El’tsov & I. N. Ganebnykh

  5. Postovskii Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, ul. S. Kovalevskoi/Akademicheskaya 22/20, Yekaterinburg, 620990, Russia

    I. N. Ganebnykh

Authors
  1. P. P. Mukovoz
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  2. V. A. Andreeva
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  3. V. O. Koz’minykh
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  4. O. S. El’tsov
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  5. I. N. Ganebnykh
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  6. E. N. Koz’minykh
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Corresponding author

Correspondence to P. P. Mukovoz.

Additional information

Original Russian Text © P.P. Mukovoz, V.A. Andreeva, V.O. Koz’minykh, O.S. El’tsov, I.N. Ganebnykh, E.N. Koz’minykh, 2016, published in Zhurnal Organicheskoi Khimii, 2016, Vol. 52, No. 1, pp. 9–12.

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Mukovoz, P.P., Andreeva, V.A., Koz’minykh, V.O. et al. Synthesis and structural peculiarities of disodium 1,6-dioxoalka-2,4-diene-3,4-diolates. Russ J Org Chem 52, 1–4 (2016). https://doi.org/10.1134/S1070428016010012

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  • DOI: https://doi.org/10.1134/S1070428016010012

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