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A Novel Carbon Paste Electrode-Modified Electrocatalytic CO–Ce–NPs for Sulfite Detection: A Sonochemical Synthesis

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Abstract

The present study introduced a novel ion-pair complex of [Co(5,5´-dmbpy)3][Ce(NO3)6] (a1) fabricated by the reaction of Co(NO3)2·6H2O, Ce(NO3)3·6H2O, NaNO3 and 5,5´-dimethyl-2,2´-bipyridine ligand. A sonochemical method was used to synthesize the nano-scale [Co(5,5´-dmbpy)3][Ce(NO3)6] (a2). The sulfite was then detected and quantified on a carbon paste electrode (CPE) modified with ferrocene derivative and cobalt nanoparticles (Co-NPs). Scanning electron microscopy (SEM) and X-ray powder diffraction (XRD) were employed to characterize the Co-NPs. The results showed a significant improvement in the electrocatalytic activity and electro-active surface area following the CPE surface modification with the ferrocene derivative and Co-NPs. The voltammetric detection of sulfite was performed successfully by the as-fabricated sensor in real samples, with the linear dynamic range and the limit of detection of 0.07–440.0 and 0.03 µM, under optimal conditions, respectively.

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Acknowledgements

We sincerely thank the University of Sistan and Baluchestan, Kerman University of Medical Sciences, Kerman Institute of Science and High Technology and Environmental Sciences, University of Parma, Parco Area delle Scienze Parma, Italy, for providing financial support for this work.

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The authors received no financial support for the research, authorship, and publication of this article.

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Authors and Affiliations

  1. Department of Chemistry, University of Sistan and Baluchestan, P.O. Box 98135-674, Zahedan, Iran

    Tahere Kondori & Niloufar Akbarzadeh-T

  2. Research Center for Tropical and Infectious Diseases, Kerman University of Medical Sciences, Kerman, Iran

    Somayeh Tajik

  3. Environment Department, Institute of Science and High Technology and Environmental Sciences, Graduate University of Advanced Technology, Kerman, Iran

    Hadi Beitollahi

  4. Department of Organic Chemistry, Faculty of Chemistry, University of Mazandaran, Babolsar, Iran

    Rahman Hosseinzadeh

  5. School of Public Health, Bam University of Medical Sciences, Bam, Iran

    Farideh Mousazadeh

  6. Department of Chemistry, Payame Noor University, Tehran, Iran

    Sayed Zia Mohammadi

  7. Department of Chemistry, Life Sciences and Environmental Sustainability, University of Parma, Parco Area delleScienze 17/A, 43124, Parma, Italy

    Cloudia Graiff

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  1. Tahere Kondori
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  2. Somayeh Tajik
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  3. Niloufar Akbarzadeh-T
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  5. Rahman Hosseinzadeh
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  6. Farideh Mousazadeh
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  7. Sayed Zia Mohammadi
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  8. Cloudia Graiff
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Correspondence to Somayeh Tajik or Niloufar Akbarzadeh-T.

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Kondori, T., Tajik, S., Akbarzadeh-T, N. et al. A Novel Carbon Paste Electrode-Modified Electrocatalytic CO–Ce–NPs for Sulfite Detection: A Sonochemical Synthesis. Iran J Sci Technol Trans Sci 46, 1387–1398 (2022). https://doi.org/10.1007/s40995-022-01345-y

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