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Sr and Pb Isotopic Compositions in Dolostones of the Lower Riphean Billyakh Group, Anabar Uplift: Step-Leaching Technique in Chemostratigraphy and Geochronology

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Abstract—

This paper presents new age estimates and results obtained by the chemostratigraphic study of dolostones of the Billyakh Group, which consists of the Kotuikan and the Yusmastakh formations. The Billyakh Group forms the upper part of the Riphean section of the Anabar uplift in northern Siberia. The stepwise dissolution technique was used for the first time to determine the 87Sr/86Sr, 206Pb/204Pb, and 207Pb/204Pb isotopic ratios in dolostones. The Rb‒Sr systematics was studied by the chemical removal of about a third of the crushed sample (fraction L1) by the preliminary acid leaching in 0.2 N CH3COOH and the subsequent partial dissolution (fraction L2) of the remaining part of the sample in CH3COOH with the same concentration. The Pb‒Pb isotope systematics of dolostones was studied by the six-step dissolution of crushed samples in 0.5 N HBr. These procedures led to the removal of secondary carbonate material and greatly improved the quality of Sr chemostratigraphic and geochronological information. The initial 87Sr/86Sr ratios of the least altered carbonate material (fraction L2) of the Billyakh Group dolostones are 0.70502 ± 0.00029 in the Kotuikan Formation, 0.70519 ± 0.00026 in the lower subformation of the Yusmastakh Formation, and 0.70511 ± 0.00018 in the upper subformation of the Yusmastakh Formation. The Pb‒Pb age of early diagenesis of Kotuikan and Yusmastakh dolostones (1519 ± 18 Ma at MSWD = 1.8) was calculated from the results obtained for carbonate fractions L3–L6. Secondary carbonate fractions L1‒L2 are characterized by a Pb‒Pb age of 1466 ± 54 Ma at MSWD = 0.6. The δ13C values vary from ‒1 to ‒0.4‰ in dolostones of the Kotuikan Formation and from ‒0.4 to +0.8‰ in those of the Yusmastakh Formation (from ‒0.1 to +0.4‰ in the lower subformation and from ‒0.4 to +0.8‰ in the upper subformation). Comparison of these variations, as well as variations in the initial 87Sr/86Sr ratios in dolostones of the Kotuikan Formation and the Lower and Upper Yusmastakh subformations (0.70460‒0.70499, 0.70450‒0.70525, and 0.70462‒0.70523, respectively), does not make it possible to distinguish these units on the basis of chemostratigraphic characteristics.

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ACKNOWLEDGMENTS

We thank E.M. Prasolov (Center for Isotopic Research, Karpinsky Russian Geological Research Institute, St. Petersburg), who participated in the determination of C and O isotopic compositions in dolostones, and A.A. Ryasnyi (Karpinsky Russian Geological Research Institute, St. Petersburg) for help in the lithological and petrographic study of dolostones, as well as T.L. Turchenko and O.L. Galankina (Institute of Precambrian Geology and Geochronology, Russian Academy of Sciences) for providing the data on chemical and mineralogical compositions of the insoluble noncarbonate component of dolostones. We are grateful to A.B. Kotov and S.I. Shkolnik for favorable reviews and useful suggestions which contributed to the improvement of this paper.

Funding

The work was supported by the Russian Science Foundation (project no. 18-17-00247-P).

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Authors and Affiliations

  1. Institute of Precambrian Geology and Geochronology, Russian Academy of Sciences, 199034, St. Petersburg, Russia

    I. M. Gorokhov, A. B. Kuznetsov, I. M. Vasil’eva, G. V. Konstantinova & N. G. Rizvanova

  2. Institute of Geology of Ore Deposits, Petrography, Mineralogy, and Geochemistry, Russian Academy of Sciences, 119017, Moscow, Russia

    E. O. Dubinina

  3. Karpinsky Russian Geological Research Institute, 199106, St. Petersburg, Russia

    G. V. Lipenkov

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Correspondence to I. M. Gorokhov.

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Reviewers: A.B. Kotov and S.I. Shkolnik

Translated by E. Maslennikova

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Gorokhov, I.M., Kuznetsov, A.B., Vasil’eva, I.M. et al. Sr and Pb Isotopic Compositions in Dolostones of the Lower Riphean Billyakh Group, Anabar Uplift: Step-Leaching Technique in Chemostratigraphy and Geochronology. Stratigr. Geol. Correl. 30, 201–227 (2022). https://doi.org/10.1134/S0869593822040049

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