Evolution of the microstructure of steel 110G13L under friction is studied using the method of synchrotron x-ray diffraction and subsequent profile analysis of the diffraction peaks. Friction of the high-manganese steel is accompanied by accumulation of crystal lattice defects, which finds reflection in changes in the full widths of half maximums. The experimentally determined structural defects are a result of growth of microdistortions of the austenite lattice and reduction of the sizes of coherent scattering domains. It is shown that the friction interaction produces anisotropic displacement of the diffraction maximums of the austenite, which indicates enhanced probability of formation of stacking faults and lowering of the stacking fault energy. Obvious features of mechanically induced phase transformations have not been detected.
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A. A. Yeleussizova, M. K. Skakov, A. M. Zhilkashinova, and O. V. Rofman, “Deformation twinning in hadfield steel,” Adv. Mater. Res., 772, 62 – 67 (2013) (https://doi.org/10.4028/www.scientific.net/AMR.772.62).
Yu. F. Ivanov, E. A. Aleshina, E. A. Kolubaev, et al., ‘Laws of structure formation in the surface layer of Hadfield steel under friction,” Fiz. Mezomekh., 9, 83 – 90 (2006).
V. E. Gromov, Yu. F. Ivanov, R. S. Qin, et al., “Degradation of structure and properties of rail surface layer at long-term operation,” Mater. Sci. Technol., 33, 1473 – 178 (2017) (https://doi.org/10.1080/02670836.2017.1287983).
K. G. Rowe, A. I. Bennett, B. A. Krick, and W. G. Sawyer, “In situ thermal measurements of sliding contacts,” Tribol. Int., 62, 2080214 (2013) (https://doi.org/10.1016/j.triboint.2013.02.028).
Y. Matsuzaki, K. Yagi, and J. Sugimura, “In-situ fast and long observation system for friction surfaces during scuffing of steel,” Wear, 386 – 387, 15 – 172 (2017) (https://doi.org/10.1016/j.wear.2017.06.013).
D. V. Lychagin, A. V. Filippov, E. A. Kolubaev, et al., “Dry sliding of Hadfield steel single crystal oriented to deformation by slip and twinning: Deformation, wear, and acoustic emission characterization,” Tribol. Int., 119, 1 – 18 (2018) (https://doi.org/10.1016/j.triboint.2017.10.027).
Y. Muramatsu, M. Okuyama, N. Takahashi, et al., “Newly developed friction tester for in situ soft x-ray absorption measurements of frictional engine-oil/metals interfaces,” Anal. Sci., 33, 1465 – 1468 (2017) (https://doi.org/https://doi.org/10.2116/analsci.33.1465).
K. Yagi, Y. Ebisu, J. Sugimura, et al., “In situ observation of wear process before and during scuffing in sliding contact,” Tribol. Lett., 43, 361 – 368 (2011) (https://doi.org/10.1007/s11249-011-9817-3).
K. Yagi, T. Izumi, J. Koyamachi, et al., “In situ observation of crystal grain orientation during scuffing process of steel surface using synchrotron x-ray diffraction,” Tribol. Lett., 68, 1 – 15 (2020) (https://doi.org/10.1007/s11249-020-01357-y).
I. A. Bataev, D. V. Lazurenko, A. A. Bataev, et al., “A novel operando approach to analyze the structural evolution of metallic materials during friction with application of synchrotron radiation,” Acta Mater., 196, 355 – 369 (2020) (https://doi.org/10.1016/j.actamat.2020.06.049).
R. Davies, M. Burghammer, and C. Riekel, An Overview of the ESRF’s ID13 Microfocus Beamline (2006) (http://refhub.elsevier.com/S2214-7853(19)34151-3/h0080).
B. E. Warren, “X-ray studies of deformed metals,” Progr. Met. Phys., 8, 147 – 202 (1959) (https://doi.org/10.1016/0502-8205(59)90015-2).
K. I. Emurlaev, I. A. Bataev, D. V. Lazurenko, et al., “Deformation- induced martensite transformation in AISI 321 stainles steel under dry friction,” Mater. Today Proc., 25, 434 – 427 (2020) (https://doi.org/10.1016/j.matpr.2019.12.140).
W. Zhang, J. Wu, Y. Wen, et al., “Characterization of different work hardening behavior in AISI 321 stainless steel and Hadfield steel,” J. Mater. Sci., 45, 3433 – 3437 (2010) (https://doi.org/10.1007/s10853-010-4369-8).
D. Rafaja, C. Krbetschek, C. Ullrich, et al., “Stacking fault energy in austenitic steels determined by using in situ x-ray diffraction during bending,” J. Appl. Crystallogr., 47, 936 – 947 (2014) (https://doi.org/10.1107/S1600576714007109).
The study has been performed with financial support of the Russian Foundation for Basic Research and of the Novosibirsk Region within scientific project No. 19-48-543022 with the use of the equipment of the common access center “Structure, Mechanical and Physical Properties of Materials” (No. 13.TsKP.21.003) of the Novosibirsk State Technical University.
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Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 12, pp. 54 – 58, December, 2021.
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Emurlaev, K.I., Ognev, A.Y. & Bataev, I.A. Operando Study of Structural Changes in High-Manganese Steel Under Dry Friction. Met Sci Heat Treat 63, 688–691 (2022). https://doi.org/10.1007/s11041-022-00749-2
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DOI: https://doi.org/10.1007/s11041-022-00749-2