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Determination of Deltamethrin in Water Samples Using Sulfur and Nitrogen Co-Doped Carbon Quantum Dots as a Chemiluminescence Probe

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Abstract

The application of sulfur and nitrogen co-doped carbon quantum dot−potassium permanganate chemiluminescence (CL) system for the determination of trace amounts of deltamethrin insecticide was investigated. The results showed that traces of deltamethrin significantly increased the CL of this system in the optimized conditions. This increase was proportional to the concentration of deltamethrin and was used for its determination. We prepared sulfur and nitrogen co-doped carbon quantum dots by hydrothermal method and characterized by fluorescence, X-ray and infrared spectra and transmission electron microscopy. In the optimum analytical conditions, the calibration graph was linear in the range of 1.8 to 20.0 µg/L with a detection limit of 0.3 µg/L. The new tested method has simple set up, high sensitivity and has been successfully applied to the determination of deltamethrin in water samples.

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REFERENCES

  1. Yan, X., Li, H., and Su, X., TrAC, Trends. Anal. Chem., 2018, vol. 103, p. 1.

    Article  CAS  Google Scholar 

  2. Fereja, T.H., Hymete, A., and Gunasekaran, T., ISRN Spectrosc., 2013, vol. 2013, p. 1.

    Article  Google Scholar 

  3. Nsibande, S.A. and Forbes, P.B.C., Anal. Chim. Acta, 2016, vol. 945, p. 9.

    Article  CAS  Google Scholar 

  4. Isacsson, U. and Wettermark, G., Anal. Chim. Acta, 1974, vol. 68, no. 2, p. 339.

    Article  CAS  Google Scholar 

  5. Amjadi, M., Manzoori, J.L., Hallaj, T., and Sorouraddin, M.H., Microchim. Acta, 2014, vol. 181, nos. 5–6, p. 671.

    Article  CAS  Google Scholar 

  6. Zhang, H.Y., Wang, Y., Xiao, S., Wang, H., Wang, J.H., and Feng, L., Biosens. Bioelectron., 2017, vol. 87, p. 46.

    Article  CAS  Google Scholar 

  7. Amjadi, M., Manzoori, J.L., and Hallaj, T., J. Lumin., 2015, vol. 158, p. 160.

    Article  CAS  Google Scholar 

  8. Li, H., Shao, F.Q., Zou, S.Y., Yang, Q.J., Huang, H., Feng, J.J., and Wang, A.J., Microchim. Acta, 2016, vol. 183, no. 2, p. 821.

    Article  CAS  Google Scholar 

  9. Liu, B. and Han, S., Microchim. Acta, 2016, vol. 183, no. 11, p. 3087.

    Article  CAS  Google Scholar 

  10. Cui, X., Wang, Y., Liu, J., Yang, Q., Zhang, B., Gao, Y., Wang, Y., and Lu, G., Sens. Actuators, B, 2017, vol. 242, p. 1272.

    Article  CAS  Google Scholar 

  11. Zou, S., Hou, C., Fa, H., Zhang, L., Ma, Y., Dong, L., Li, Dan., Huo, D., and Yang, M., Sens. Actuators, B, 2017, vol. 239, p. 1033.

    Article  CAS  Google Scholar 

  12. Zhang, Y., Wang, Y., Feng, X., Zhang, F., Yang, Y., and Liu, X., Appl. Surf. Sci., 2016, vol. 387, p. 1236.

    Article  CAS  Google Scholar 

  13. Lin, Y., Yao, B., Huang, T., Zhang, S., Cao, X., and Weng, W., Microchim. Acta, 2016, vol. 183, no. 7, p. 2221.

    Article  CAS  Google Scholar 

  14. Hallaj, T., Amjadi, M., Manzoori, J.L., and Azizi, N., Luminescence, 2017, vol. 32, no. 7, p. 1174.

    Article  CAS  Google Scholar 

  15. Lau, C., Lu, J., and Kai, M., Anal. Chim. Acta, 2004, vol. 503, no. 2, p. 235.

    Article  CAS  Google Scholar 

  16. Lu, J., Lau, C., Lee, M.K., and Kai, M., Anal. Chim. Acta, 2002, vol. 455, no. 2, p. 193.

    Article  CAS  Google Scholar 

  17. Amjadi, M., Manzoori, J.L., Hallaj, T., and Sorouraddin, M.H., Spectrochim. Acta, Part A, 2014, vol. 122, p. 715.

    Article  CAS  Google Scholar 

  18. Algar, W.R., Kim, H., Medintz, I.L., and Hildebrandt, N., Coord. Chem. Rev., 2014, vol. 263, p. 65.

    Article  Google Scholar 

  19. Gu, D., Shang, S., Yu, Q., and Shen, J., Appl. Surf. Sci., 2016, vol. 390, p. 38.

    Article  CAS  Google Scholar 

  20. Amjadi, M., Manzoori, J.L., Hallaj, T., and Azizi, N., J. Lumin., 2017, vol. 182, p. 246.

    Article  CAS  Google Scholar 

  21. Ge, S., Lu, J., Ge, L., Yan, M., and Yu, J., Spectrochim. Acta, Part A, 2011, vol. 79, no. 5, p. 1704.

    Article  CAS  Google Scholar 

  22. Shan, X., Chai, L., Ma, J., Qian, Z., Chen, J., and Feng, H., Analyst, 2014, vol. 139, no. 10, p. 2322.

    Article  CAS  Google Scholar 

  23. Liu, T., Cui, Z., Zhou, J., Wang, Y., and Zou, Z., Nanoscale Res. Lett., 2017, vol. 12, no. 1, p. 375.

    Article  Google Scholar 

  24. Lu, Q., Sun, Y., Ares, I., Anadón, A., Martínez, M., Martínez-Larrañaga, MR., Yuan, Z., Wang, X., and Martínez, MA., Environ. Res., 2019, vol. 170, p. 260.

    Article  CAS  Google Scholar 

  25. Kulikov, A.U., Chromatographia, 2007, vol. 66, no. 5, p. 303.

    Article  CAS  Google Scholar 

  26. Galera, M.M., García, M.D.G., and Valverde, R.S., J. Chromatogr. A, 2006, vol. 1113, no. 1, p. 191.

    Article  CAS  Google Scholar 

  27. Amin, A.S., Moalla, S.M.N., Salama, M.S.S., Ali, A., and Gouda, A.A., Int. J. Adv. Res. Chem. Sci., 2015, vol. 2, no. 10, p. 72.

    Google Scholar 

  28. Ge, S., Zhang, C., Yu, F., Yan, M., and Yu, J., Sens. Actuators. B: Chem., 2011, vol. 156, no. 1, p. 222.

    Article  CAS  Google Scholar 

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Correspondence to Jamshid L Manzoori.

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Azimi, M., Manzoori, J.L., Amjadi, M. et al. Determination of Deltamethrin in Water Samples Using Sulfur and Nitrogen Co-Doped Carbon Quantum Dots as a Chemiluminescence Probe. J Anal Chem 76, 1217–1224 (2021). https://doi.org/10.1134/S1061934821100026

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  • DOI: https://doi.org/10.1134/S1061934821100026

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