Skip to main content
Log in

Sensitivity of Strength Via Temperature for SiC/SiC Composites and SiC Fibers in an Oxygen-Free Environment

  • Published:
Applied Composite Materials Aims and scope Submit manuscript

Abstract

The sensitivity of strength via temperature for SiC/SiC composites and SiC fibers in an oxygen-free environment is studied through experimental investigation and theoretical analysis. Tensile tests are performed on SiC/SiC minicomposites at room temperature, 500 and 1000 ℃ in an oxygen-free environment. A high-efficiency method is proposed to obtain the high-temperature strength distribution of SiC fibers. The experimental results show that the sensitivity of strength via temperature is high for SiC fibers but low for SiC/SiC minicomposites. To explain this phenomenon, the strength model of minicomposites is developed. The theoretical analysis reveals that the low sensitivity of strength via temperature for minicomposites results from that the influences of the changes of the Weibull parameters m and σ0 at elevated temperatures are offset.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

Data Availability

The datasets generated during and analysed during the current study are available from the corresponding author on reasonable request.

References

  1. Lamon, J.: Review: creep of fibre-reinforced ceramic matrix composites. Int. Mater. Rev. 65(1), 28–62 (2020)

    Article  CAS  Google Scholar 

  2. Zok, F.W., Maxwell, P.T., Kawanishi, K., et al.: Degradation of a SiC-SiC composite in water vapor environments. J. Am. Ceram. Soc. 103(3), 1927–1941 (2019)

    Article  Google Scholar 

  3. Guo, S., Kagawa, Y.: Tensile fracture behavior of continuous SiC fiber-reinforced SiC matrix composites at elevated temperatures and correlation to in situ constituent properties. J. Eur. Ceram. Soc. 22(13), 2349–2356 (2002)

    Article  CAS  Google Scholar 

  4. Jing, X., Shi, D., Yang, X., et al.: Fiber strength measurement for KD-I(f)/SiC composites and correlation to tensile mechanical behavior at room and elevated temperatures. Ceram. Int .41(1), 299–307 (2015)

    Article  Google Scholar 

  5. Zhang, Y., Jiang, Y., Ren, D., et al.: High-temperature tensile behavior of 3D SiC/SiC composites. J. Phys. Conf. Ser. 1605(1), 12126 (2020)

    Article  CAS  Google Scholar 

  6. Davies, I.J., Ogasawara, T., Ishikawa, T.: Stress/strain behavior of a 3-D woven composite based on the SiC/SiC system. J. Ceram. Soc. Jpn. 109(7), 643–646 (2001)

    Article  CAS  Google Scholar 

  7. Guo, S., Kagawa, Y.: Temperature Dependence of in situ Constituent Properties of Polymer-infiltration-pyrolysis-processed Nicalon SiC Fiber-reinforced SiC Matrix Composite. J. Mater. Res. 15(4), 951–960 (2000)

    Article  CAS  Google Scholar 

  8. Guo, S., Kagawa, Y.: Temperature Dependence of Tensile Strength for a Woven Boron-Nitride-Coated Hi-Nicalon SiC Fiber-Reinforced Silicon-Carbide-Matrix Composite. J. Am. Ceram. Soc. 84(9), 2079–2085 (2001)

    Article  CAS  Google Scholar 

  9. Deng, Y., Li, W., Wang, X., et al.: Temperature-dependent tensile strength model for 2D woven fiber reinforced ceramic matrix composites. J. Am. Ceram. Soc. 101(11), 5157–5165 (2018)

    Article  CAS  Google Scholar 

  10. Kotani, M., Konaka, K., Ogihara, S.: The effect on the tensile properties of PIP-processed SiC/SiC composite of a chemical vapor-infiltrated SiC layer overlaid on the pyrocarbon interface layer. Compos. Part A Appl. Sci. Manuf. 87, 123–130 (2016)

    Article  CAS  Google Scholar 

  11. Wu, B., Ni, N., Fan, X., et al.: Strength degradation of SiC fibers with a porous ZrB2-SiC coating: Role of the coating porous structure. J. Eur. Ceram. Soc. 40(4), 961–971 (2020)

    Article  CAS  Google Scholar 

  12. Chen, Y., Chen, Z., Zhang, R., et al.: Structural evolution and mechanical properties of Cansas-III SiC fibers after thermal treatment up to 1700 °C. J. Eur. Ceram. Soc. 41(10), 5036–5045 (2021)

    Article  CAS  Google Scholar 

  13. Cao, S., Wang, J., Wang, H.: Effect of heat treatment on the microstructure and tensile strength of KD-II SiC fibers. Mater. Sci. Eng. A 673, 55–62 (2016)

    Article  CAS  Google Scholar 

  14. Cao, S., Wang, J., Wang, H.: High-temperature behavior and degradation mechanism of SiC fibers annealed in Ar and N2 atmospheres. J. Mater. Sci. 51(9), 4650–4659 (2016)

    Article  CAS  Google Scholar 

  15. Zhao, C., Wang, Y., Zhang, G., et al.: Effect of heat treatment on the microstructure and properties of CVD SiC fiber. J. Mater. Sci. Technol. 33(11), 1378–1385 (2017)

    Article  CAS  Google Scholar 

  16. Zhang, S., Gao, X., Dong, H., et al.: In situ modulus and strength of carbon fibers in C/SiC composites. Ceram. Int. 43(9), 6885–6890 (2017)

    Article  CAS  Google Scholar 

  17. Pysher, D.J., Goretta, K.C., Hodder, R.S., et al.: Strengths of ceramic fibers at elevated temperatures. J. Am. Ceram. Soc. 72(2), 284–288 (1989)

    Article  CAS  Google Scholar 

  18. Almansour, A., Maillet, E., Ramasamy, S., et al.: Effect of fiber content on single tow SiC minicomposite mechanical and damage properties using acoustic emission. J. Eur. Ceram. Soc. 35, 3389–3399 (2015)

    Article  CAS  Google Scholar 

  19. Dai, J., Wang, Y., Xu, Z., et al.: Effect of BN/SiC interfacial coatings on the tensile properties of SiC/SiC minicomposites fabricated by PIP. Ceram. Int. 46(16), 25058–25065 (2020)

    Article  CAS  Google Scholar 

  20. Lu, Z., Yue, J., Fu, Z., et al.: Microstructure and mechanical performance of SiCf/BN/SiC mini-composites oxidized at elevated temperature from ambient temperature to 1500 °C in air. J. Eur. Ceram. Soc. 40(8), 2821–2827 (2020)

    Article  CAS  Google Scholar 

  21. Loidl, D., Paris, O., Rennhofer, H., et al.: Skin-core structure and bimodal Weibull distribution of the strength of carbon fibers. Carbon. 45(14), 2801–2805 (2007)

    Article  CAS  Google Scholar 

  22. Nemeth, N., Walker, A., Baker, E., et al.: Large-scale Weibull analysis of H-451 nuclear-grade graphite rupture strength. Carbon. 58, 208–225 (2013)

    Article  CAS  Google Scholar 

  23. Naik, D.L., Fronk, T.H.: Weibull distribution analysis of the tensile strength of the kenaf bast fiber. Fiber. Polym. 17(10), 1696–1701 (2016)

    Article  CAS  Google Scholar 

  24. Guo, M., Zhang, T.H., Chen, B.W., et al.: Tensile strength analysis of palm leaf sheath fiber with Weibull distribution. Compos. Part A Appl. Sci. Manuf. 62, 45–51 (2014)

    Article  CAS  Google Scholar 

  25. Sakin, R., Ay, İ: Statistical analysis of bending fatigue life data using Weibull distribution in glass-fiber reinforced polyester composites. Mater. Design. 29(6), 1170–1181 (2008)

    Article  CAS  Google Scholar 

  26. Gao, X., Zhang, S., Fang, G., et al.: Distribution of slip regions on the fiber-matrix interface of ceramic matrix composites under arbitrary loading. J. Reinf. Plast. Comp. 34(20), 1713–1723 (2015)

    Article  CAS  Google Scholar 

  27. Han, X., Gao, X., Song, Y.: Effect of heat treatment on the microstructure and mechanical behavior of SiC/SiC mini-composites. Mat. Sci. Eng. A-Struct. 746, 94–104 (2019)

    Article  CAS  Google Scholar 

  28. Mei, H., Li, H., Bai, Q., et al.: Increasing the strength and toughness of a carbon fiber/silicon carbide composite by heat treatment. Carbon. 54, 42–47 (2013)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This work was supported by the National Natural Science Foundation of China [grant numbers 51675266, 11972183]; China Postdoctoral Science Foundation [grant number 2021M691566]; and Jiangsu Planned Projects for Postdoctoral Research Funds.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Sheng Zhang.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Zhang, S., Meng, W. & Zhang, Z. Sensitivity of Strength Via Temperature for SiC/SiC Composites and SiC Fibers in an Oxygen-Free Environment. Appl Compos Mater 28, 1979–1995 (2021). https://doi.org/10.1007/s10443-021-09961-4

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10443-021-09961-4

Keywords

Navigation