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A 3D SUPRAMOLECULAR POLYMER INVOLVING HYDROGEN BONDS BASED ON NICKEL(II), 1,3-BENZENEDICARBOXYLIC ACID, AND A NITROGEN-CONTAINING LIGAND

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Abstract

The [Ni(1,3-bdc)(L)(H2O)2]n·2nH2O (1) coordination polymer (1,3-H2bdc = 1,3-benzenedicarboxylic acid, L = 4,4′-N,N′-bis(3-pyridylformamide)diphenyl ether) is hydrothermally synthesized and structurally characterized by single crystal X-ray diffraction and UV-Vis spectroscopy. The single crystal X-ray diffraction analysis reveals that each nickel(II) atom is six-coordinated with one 1,3-bdc anion, one L ligand, two coordinated and two free water molecules. The one-dimensional chain of complex 1 is formed by Ni metal and mixed ligands with a Ni⋯Ni distance of 7.780 Å. Furthermore, the existence of strong hydrogen bonding between chains and layers forms a final three-dimensional supramolecular structure. The UV-Vis spectroscopy of the title complex is briefly investigated. Thermal behavior is also examined.

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Funding

The authors are thankful for the financial support of this research work from the National Natural Science Foundation of China (No. 21607051) and the Graduate Innovation Project of Jilin Normal University (No. 202030).

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Authors and Affiliations

  1. Key Laboratory of Preparation and Applications of Environmental Friendly Materials, Jilin Normal University, Ministry of Education, Changchun, People’s Republic of China

    Y. Song, G. T. Li & X. Y. Wang

  2. Key Laboratory of Functional Materials Physics and Chemistry of the Ministry of Education, Jilin Normal University, Ministry of Education, Changchun, People’s Republic of China

    Y. Song, G. T. Li & X. Y. Wang

  3. Department of Chemistry, Jilin Normal University, Siping, People’s Republic of China

    Y. Song, L. P. Xu, G. T. Li & X. Y. Wang

Authors
  1. Y. Song
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  2. L. P. Xu
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  3. G. T. Li
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  4. X. Y. Wang
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Correspondence to X. Y. Wang.

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Text © The Author(s), 2021, published in Zhurnal Strukturnoi Khimii, 2021, Vol. 62, No. 7, pp. 1182-1188.https://doi.org/10.26902/JSC_id74462

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Song, Y., Xu, L.P., Li, G.T. et al. A 3D SUPRAMOLECULAR POLYMER INVOLVING HYDROGEN BONDS BASED ON NICKEL(II), 1,3-BENZENEDICARBOXYLIC ACID, AND A NITROGEN-CONTAINING LIGAND. J Struct Chem 62, 1105–1111 (2021). https://doi.org/10.1134/S0022476621070155

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