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Magnetic Properties and Structure of the Alloy Fe63.5Ni10Cu1Nb3Si13.5B9 with Induced Magnetic Anisotropy

  • ELECTRICAL AND MAGNETIC PROPERTIES
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Abstract

In the alloy Fe63.5Ni10Cu1Nb3Si13.5B9, which is conventional FINEMET with Fe replaced by 10 at % Ni, the effects of the temperature and time of nanocrystallizing annealing in the presence of tensile stresses (stress annealing, SA) on the magnetic properties, magnetic anisotropy, and structure are considered. In the entire studied SA temperature range (480–550°С), induced magnetic anisotropy (IMA) of the easy-plane type occurs in the studied alloy. The tensile stresses upon SA were 200 MPa. In the course of SA at the minimum temperature, anisotropy with the minimum IMA constant (200 J/m3) is induced. The maximum SA duration, i.e., 4 h, is required. At SA temperatures of 540–550°С, 10 min is sufficient to induce IMA with the maximum constant ~2000 J/m3. It is shown that the structural state (phase composition) is correlated with the magnetic properties and IMA. Thus, the increase in the coercivity with an increase in the SA duration at 540–550°С (as well as at 520°С) is due to the development of the tetragonal phase in the alloy. The α‑(Fe,Ni)Si solid solution and Fe3Si phases form upon treatment for 10 min. The decrease in the IMA constant with an increase in the SA time at 540–550°С from 10 min to 1 h is most likely due to the change in the volume fractions of the structural components of the alloy with negative and positive magnetostriction.

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REFERENCES

  1. N. A. Skulkina, O. A. Ivanov, A. K. Mazeeva, P. A. Kuznetsov, E. A. Stepanova, O. V. Blinova, and E. A. Mikhalitsyna, “Magnetization processes in ribbons of soft magnetic amorphous alloys,” Phys. Met. Metallogr. 119, No. 2, 127–133 (2018).

    Article  CAS  Google Scholar 

  2. N. V. Dmitrieva, V. A. Lukshina, E. G. Volkova, B. N. Filippov, and A. P. Potapov, “Magnetic properties and thermal stability of the soft magnetic alloy (Fe0.7Co0.3)88Hf4Mo2Zr1B4Cu1 nanocrystallized in the presence of an alternating magnetic field,” Phys. Met. Metallogr. 118, No. 10, 946–953 (2017).

    Article  CAS  Google Scholar 

  3. V. S. Tsepelev, Yu. N. Starodubtsev, V. A. Zelenin, V. A. Kataev, V. Ya. Belozerov, and V. V. Konashkov, Dilatometric analysis of the process of the nanocrystallization of Fe72.5Cu1Nb2Mo1.5Si14B9 soft magnetic alloy,” Phys. Met. Metallogr. 118, No. 6, 553–557 (2017).

    Article  CAS  Google Scholar 

  4. E. A. Stepanova, S. O. Volchkov, V. A. Lukshina, D. A. Shishkin, D. M. Khudyakova, A. Larrañaga, and G. V. Kurlyandskaya, “Structure, magnetic properties and magnetic impedance of fast quenched ribbons of alloys based on FINEMET in the initial state and after heat treatment, Phys. Met. Metallogr. 121, No. 10, 961–967 (2020).

    Article  CAS  Google Scholar 

  5. D. A. Bukreev, M. S. Derevyanko, A. A. Moiseev, A. S. Kuz’mina, G. V. Kurlyandskaya, A. V. Semirov, “Magnetic properties and high-frequency impedance of nanocrystalline FeSiBNbCu ribbons in a 300 to 723 K temperature range,” Phys. Met. Metallogr. 121, No. 10, 949–954 (2020).

    Article  CAS  Google Scholar 

  6. P. Agudo and M. Vazguez, “Influence of Ni on structural and magnetic properties of Fe73.5 – xNixSi13.5B9Nb3Cu1 (0 ≤ x ≤ 25) alloys,” J. Appl. Phys. 97, 023901 (2005).

    Article  Google Scholar 

  7. P. Duhaj, P. Švec, J. Sitec, and D. Janičkovič, “Thermodinamic, kinetic and structural aspects of the formation of nanocrystalline phases in Fe73.5 – xNixCu1Nb3Si13.5B9 alloys,” Mater. Sci. Eng., A 304–306, 178–186 (2001).

    Article  Google Scholar 

  8. V. A. Kataev, Yu. N. Starodubtsev, E. A. Mikhalitsyna, V. Ya. Belozerov, and R. V. Tsyngalov, “Mproperties and induced anisotropy of nanocrystalline Fe72.5 – xNixCu1.1Nb1.9Mo1.5Si14.3B8.7 alloys,” Phys. Met. Metallogr. 118, No. 6, 558–563 (2017).

    Article  CAS  Google Scholar 

  9. Y. Yoshizawa, S. Fujii, D. H. Ping, M. Ohnuma, and K. Hono, “Magnetic properties of nanocrystalline FeMCuNbSiB alloys (M: Co, Ni),” Scr. Mater. 48, 863–868 (2003).

    Article  CAS  Google Scholar 

  10. Y. Y. Jia, Z. Wang, R-M. Shi, J. Yang, H-J. Kang, and T. Lin, “Influence of Ni addition on structure and magnetic properties of FeCo-based Finemet-type alloys,” J. Appl. Phys. 109, 073917 (2011).

    Article  Google Scholar 

  11. N. Iturriza, L. Fernandez, M. Ipatov, G. Vara, A. R. Pierna, J. J. del Val, A. Chizhik, and J. Conzalez, “Nanostructure and magnetic properties of Ni-substituted finemet ribbons,” J. Magn. Magn. Mater. 316, e74–e77 (2007).

    Article  CAS  Google Scholar 

  12. V. A. Lukshina, N. V. Dmitrieva, E. G. Volkova, and D. A. Shishkin, “Magnetic properties of the Fe63.5Ni10Cu1Nb3Si13.5B9 alloy nanocrystallized in the presence of tensile stresses,” Phys. Met. Metallogr. 120, No. 4, 320 (2019).

    Article  CAS  Google Scholar 

  13. V. A. Lukshina, N. V. Dmitrieva, E. G. Volkova, and D. A. Shishkin, “Structure of the Fe63.5Ni10Cu1Nb3Si13.5B9 alloy nanocrystallized in the presence of tensile stresses,” Phys. Met. Metallogr. 120, No. 12, 1145–1151 (2019).

    Article  CAS  Google Scholar 

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Funding

The work was partially supported by the State Assignment of the Ministry of the Education and Science (theme “Magnet” No. АААА-А18-118020290129-5) and the Ural Branch of Russian Academy of Sciences (UB RAS) (project no. 18-10-2-5). The electron-microscopy study was performed in the electron-microscopy center of the Testing Center of Nanotechnology and Advanced Materials Center for Collective Use of the Miheev Institute of Metal Physics UB RAS.

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Authors and Affiliations

  1. Mikheev Institute of Metal Physics, Ural Branch, Russian Academy of Sciences, 620108, Ekaterinburg, Russia

    V. A. Lukshina, N. V. Dmitrieva, E. G. Volkova & D. A. Shishkin

  2. Ural Federal University, 620002, Ekaterinburg, Russia

    V. A. Lukshina & D. A. Shishkin

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  1. V. A. Lukshina
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  2. N. V. Dmitrieva
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  3. E. G. Volkova
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  4. D. A. Shishkin
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Correspondence to V. A. Lukshina.

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Translated by O. Golovnya

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Lukshina, V.A., Dmitrieva, N.V., Volkova, E.G. et al. Magnetic Properties and Structure of the Alloy Fe63.5Ni10Cu1Nb3Si13.5B9 with Induced Magnetic Anisotropy. Phys. Metals Metallogr. 122, 533–539 (2021). https://doi.org/10.1134/S0031918X21060077

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