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High Temperature Oxidation Kinetics of Shot-Peened and Laser-Shock Peened Ti-Beta-21S

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Abstract

Isothermal oxidation tests of mechanically treated Ti-Beta-21S (TIMET, Ti–15Mo–3Nb–3Al–2Si, ASTM Grade 21) were performed under dry air at 650, 700 and 750 °C for 100 h and compared to untreated samples. Two different mechanical surface treatments were used: ultrasonic shot-peening (SP) and laser-shock peening (LSP). The study investigates the effect of both treatments on the oxidation kinetics of the process and the role of atmospheric nitrogen insertion. With this aim, oxidation experiments were also performed under pure oxygen. The results show that the oxidation is governed by diffusion after a short transient time. Both SP and LSP treatments improve the high temperature oxidation resistance of Ti-Beta-21S in dry air, but not in pure oxygen. The formation of a nitrogen-enriched layer at the oxide–metal interface, which is promoted by the mechanical surface treatments, explains the increase in the oxidation resistance in air by slowing down the diffusion of oxygen into the metal.

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Acknowledgements

Authors acknowledge greatly Burgundy Regional Council (BRC) and the Agglomeration Council of Chalon City for their financial contribution in SEM at Chalon sur Saône, and the PIMM Laboratory (HESAM University) and the Charles Delaunay Institute (University of Technology of Troyes) for the mechanical treatments. This work was supported by the EIPHI Graduate School (Contract ANR17-EURE-0002).

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  1. Laboratoire Interdisciplinaire Carnot de Bourgogne, UMR 6303, CNRS - Université Bourgogne Franche-Comté, 9 Avenue A. Savary, BP 47 870, 21078, Dijon Cedex, France

    V. Optasanu, M. C. Marco de Lucas, A. Kanjer, B. Vincent, T. Montesin & L. Lavisse

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  1. V. Optasanu
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  2. M. C. Marco de Lucas
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  3. A. Kanjer
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  4. B. Vincent
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  5. T. Montesin
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  6. L. Lavisse
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Correspondence to V. Optasanu.

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Optasanu, V., de Lucas, M.C.M., Kanjer, A. et al. High Temperature Oxidation Kinetics of Shot-Peened and Laser-Shock Peened Ti-Beta-21S. Oxid Met 96, 257–270 (2021). https://doi.org/10.1007/s11085-021-10043-w

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  • DOI: https://doi.org/10.1007/s11085-021-10043-w

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