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Effects of Temperature on the Properties of Ni–Co–BN (h) Nanocomposite Coating in Jet Electrodeposition

  • NANOSCALE AND NANOSTRUCTURED MATERIALS AND COATINGS
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Abstract

Ni–Co–BN (h) nanocomposite coating was prepared by jet electrodeposition (JED) under different temperatures. The surface morphology, element composition, crystal structure, microhardness and corrosion resistance of the samples prepared at different temperatures were analyzed and characterized by scanning electron microscope (SEM), energy dispersive spectrometer (EDS), X-ray diffraction (XRD), microhardness tester, electrochemical workstation, respectively. The experimental results showed that the micro-protrusions on the sample surface gradually changed from spherical to diamond with the variation of the temperature, and the consistency of the micro-protrusions was improved. The coating thickness and the Co content of the samples first increased and then decreased with the change of the temperature. The deposition temperature changed the gain size of the samples, but it had no obvious effect on the crystal structure. The crystal structure of all the samples was still face centered cubic (fcc) structure. When the temperature was 60°C, the sample had better performances in the microhardness and the corrosion resistance. Under this parameter, the average value of the microhardness reached 608.5 HV0.05, the corrosion current density was 0.54 μA/cm2, and the corrosion rate was 6.51 μm/year.

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Funding

This work was supported by Research Team of Anhui Provincial Education Department (2016SCXPTTD), Key projects of Natural Science Research of Anhui Provincial Department of Education (KJ2019A0674), Natural Science Foundation of Anhui Province (2008085ME150) and Key Discipline of Material Science and Engineering of Suzhou University (2017XJZDXK3).

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Authors and Affiliations

  1. College of Mechanical and Electrical Engineering, Suzhou University, 234000, Suzhou, Anhui, China

    Hengzheng Li, Guangzhen Zhao, Yanjiang Li, Conghu Liu, Li Li & Guang Zhu

  2. Key Laboratory of Spin Electron and Nanomaterials of Anhui Higher Education Institutes, Suzhou University, 234000, Suzhou, Anhui, China

    Hengzheng Li, Guangzhen Zhao, Yanjiang Li, Conghu Liu, Li Li & Guang Zhu

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  1. Hengzheng Li
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  2. Guangzhen Zhao
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  3. Yanjiang Li
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  4. Conghu Liu
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  5. Li Li
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Correspondence to Guang Zhu.

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Li, H., Zhao, G., Li, Y. et al. Effects of Temperature on the Properties of Ni–Co–BN (h) Nanocomposite Coating in Jet Electrodeposition. Prot Met Phys Chem Surf 57, 535–542 (2021). https://doi.org/10.1134/S2070205121030151

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