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AFRL Additive Manufacturing Modeling Series: Challenge 4, In Situ Mechanical Test of an IN625 Sample with Concurrent High-Energy Diffraction Microscopy Characterization

  • Thematic Section: Metal Additive Manufacturing Modeling Challenge Series 2020
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Abstract

We describe 3D characterization of an additively manufactured Inconel 625 nickel-base superalloy specimen conducted during a uniaxial tension test using a suite of nondestructive x-ray techniques. High-energy diffraction microscopy in both near- and far-field modalities are employed in situ to track evolution of the material orientation and stress–strain fields at six points during the mechanical test, and these data streams are registered with micro-computed tomography reconstructions which probe the material density. This data volume was matched to a multi-modal serial sectioning characterization of the specimen taken after loading, described in this article’s companion. Twenty-eight grains which were monitored throughout the experiment were selected to form the basis for AFRL AM Modeling Series Challenge 4, Microscale Structure-to-Properties.

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Acknowledgements

DBM, WDM, MO, MNS, SPD, JVB, and PAS acknowledge support from the United States Air Force Research Laboratory (AFRL). DBM is thankful for the high-performance computer time and resources provided by the AFRL DoD Supercomputing Resource Center (DSRC) that supported HEDM reconstructions performed in this work. The authors acknowledge technical discussions and logistical support from Marie Cox (AFRL, program manager for AFRL AM Modeling Series). Edwin Schwalbach (AFRL) and Michael Groeber (Ohio State University, previously employed at AFRL) are acknowledged for technical discussions and providing the AM material. Michael Uchic (AFRL) is acknowledged for technical discussions and serial sectioning coordination. Sirina Safriet (UDRI) and Basil Blank (Pulseray) are acknowledged for help with specimen preparation. Jon Almer, Ali Mashayekhi, and Kurt Goetze (Argonne National Lab) are acknowledged for support of the beamline experiment. This research used resources of the Advanced Photon Source, a U.S. Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357.

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Authors and Affiliations

  1. Hamiltonian Group LLC, Washington DC, 20007, USA

    David B. Menasche

  2. Air Force Research Laboratory, Materials and Manufacturing Directorate, Wright-Patterson AFB, Ohio, OH, 45433, USA

    William D. Musinski, Mark Obstalecki, Megna N. Shah, Sean P. Donegan & Paul A. Shade

  3. Lawrence Livermore National Laboratory, Engineering Directorate, Livermore, CA, 94550, USA

    Joel V. Bernier

  4. Argonne National Laboratory, Advanced Photon Source, Lemont, IL, 60439, USA

    Peter Kenesei & Jun-Sang Park

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  1. David B. Menasche
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Correspondence to David B. Menasche.

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Menasche, D.B., Musinski, W.D., Obstalecki, M. et al. AFRL Additive Manufacturing Modeling Series: Challenge 4, In Situ Mechanical Test of an IN625 Sample with Concurrent High-Energy Diffraction Microscopy Characterization. Integr Mater Manuf Innov 10, 338–347 (2021). https://doi.org/10.1007/s40192-021-00218-3

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