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CRYSTAL STRUCTURE OF LITHIUM, POTASSIUM, AND CALCIUM COMPLEXES WITH β-CYCLODEXTRINE

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Abstract

Three new coordination compounds are obtained in the reaction of aqueous solutions of lithium and potassium hydroxides or calcium chloride with β-cyclodextrine. Their compositions and structures are determined by single crystal X-ray diffraction. The lithium and potassium complexes represent metal-organic coordination polymers with chain (Li) and layered (K) structures. The crystal structure of the calcium compound is a packing of discrete complexes.

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Funding

The work was supported by RFBR (project No. 18-29-04001).

Diffraction data for β-CD–Li and β-CD–K compounds were obtained using synchrotron radiation and the study was supported by the Russian Science Foundation (project No. 19-73-20087).

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Authors and Affiliations

  1. Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    E. I. Koshevoi, D. G. Samsonenko & V. P. Fedin

  2. Novosibirsk State University, Novosibirsk, Russia

    D. G. Samsonenko & V. P. Fedin

  3. National Research Center “Kurchatov Institute”, Moscow, Russia

    P. V. Dorovatovskii & V. A. Lazarenko

Authors
  1. E. I. Koshevoi
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  2. D. G. Samsonenko
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  3. P. V. Dorovatovskii
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  4. V. A. Lazarenko
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  5. V. P. Fedin
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Corresponding author

Correspondence to V. P. Fedin.

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The authors declare that they have no conflict of interests.

Additional information

Russian Text © The Author(s), 2021, published in Zhurnal Strukturnoi Khimii, 2021, Vol. 62, No. 4, pp. 617-625.https://doi.org/10.26902/JSC_id71142

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Koshevoi, E.I., Samsonenko, D.G., Dorovatovskii, P.V. et al. CRYSTAL STRUCTURE OF LITHIUM, POTASSIUM, AND CALCIUM COMPLEXES WITH β-CYCLODEXTRINE. J Struct Chem 62, 577–584 (2021). https://doi.org/10.1134/S0022476621040090

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  • DOI: https://doi.org/10.1134/S0022476621040090

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