Abstract
High-temperature baked sandstone is widely distributed in the north of Shaanxi, China. The lithology of these rocks has a significant impact on the mining of underground resources such as coal. To understand changes in its physical properties after heat treatment, yellow sandstone was heated for two hour at a constant temperature of 25, 800, 1000, 1100 or 1250 °C. Data on the glossiness, hardness and colour brightness, and surface micrographs, were obtained to study the relationship between surface characteristics and temperature. The relationship between internal structural characteristics and temperature was studied using electrical properties and nuclear magnetic resonance (NMR) spectroscopy. The results showed that below 1100 °C, glossiness and porosity increased and conductivity, hardness and colour brightness decreased, mainly due to melting of the binder. Above 1100 °C, there was melting of clay minerals, quartz and feldspar particles, resulting in a sharp increase in the brightness and hardness of yellow sandstone, a sharp decrease in porosity, and glossiness and conductivity increase rarely. Combining these results with the surface micrographs, the whole thermal change mechanism could be summarised as follows: dehydration condensation of water-bearing minerals → melting of cement → melting of quartz and feldspar particles → pyro-metamorphism.
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Abbreviations
- NMR :
-
Nuclear magnetic resonance
- T2 :
-
Transverse relaxation time
- T 2 B :
-
Volume relaxation time
- T 2 :
-
Surface relaxation time
- T 2 D :
-
Diffusion relaxation time
- HL :
-
Leeb hardness symbol
- A :
-
Starting point of T2
- B :
-
First peak of T2
- C :
-
Trough of T2
- D :
-
Final peak of T2
- E :
-
End point of T2
- K :
-
Conductivity
- \(\varphi\) :
-
Porosity
- K NMR :
-
Permeability
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Acknowledgements
This work was supported by the National Natural Science Foundation of China (grant number 41672279, 41972288).
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He Zhang: Writing – original draft, Investigation. Qiang Sun: Methodology, Conceptualization, Writing—review & editing. Hailiang Jia: Supervision, Writing—review & editing. Jishi Geng: Data curation.
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Zhang, H., Sun, Q., Geng, J. et al. Effect of high temperature on physical properties of yellow sandstone. Heat Mass Transfer 57, 1981–1995 (2021). https://doi.org/10.1007/s00231-021-03088-9
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DOI: https://doi.org/10.1007/s00231-021-03088-9