Abstract
Titanium carbide (TiC) powder was combustion-synthesized in argon from mineral ilmenite and activated carbon (C) using magnesium (Mg) as a fuel. The reactant powders were taken at FeTiO3 : C : Mg molar ratios of 1 : 1 : 3 and 1 : 1.5 : 4.5. The as-combusted products were leached with 1 M HCl at 80 or 90°C to remove byproducts and impurities. Best results (fewer impurities) were obtained for combustion products derived from FeTiO3 : C : Mg green mixtures taken at a molar ratio of 1 : 1.5 : 4.5 and subjected to acid leaching at 90°C for 150 min. After leaching, agglomerated TiC particles have a size of around 100 nm. Ilmenite mineral can be recommended as an alternative source of TiO2 for fabrication of titanium carbide powders.
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ACKNOWLEDGMENTS
We are grateful to Mr. Thomas Duncan Coyne for his kind editing the English text.
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This work was financially supported by Faculty of Science, Prince of Songkla University, under the revenue budget for fiscal year 2018.
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Rattanaphan, N., Chanadee, T. Combustion Synthesis of TiC Powders from Ilmenite Mineral and Activated Carbon. Int. J Self-Propag. High-Temp. Synth. 30, 51–54 (2021). https://doi.org/10.3103/S106138622101009X
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DOI: https://doi.org/10.3103/S106138622101009X