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Performance of Cement Mortars Containing Clay Exposed to High Temperature

  • Research Article-Earth Sciences
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Abstract

The partial substitution of ordinary Portland Cement (OPC) with clay minerals as supplementary cementitious materials has been currently considered as an effective approach for reducing the harmful environmental impact and health risks of OPC. Although cement mortars are not easily ignitable, the exposure to elevated temperatures can alter their microstructure, leading to reduction in the strength and damage. Therefore, improving the temperature resistance of the cement mortars through the incorporation of local clay minerals has been proposed in this study. The mechanical performance and physical properties of cement mortars containing Wasia Formation clay (WFC) exposed to 700 °C have been investigated. OPC was partially replaced with WFC at various mass ratios of 0, 5, 10, 15, and 20 wt%. Several methods were used to assess the physico-mechanical and structural properties such as compressive strength testing, ultrasonic pulse velocity (UPV), Schmidt hamme, scanning electron microscopy, and X-ray powder diffraction (XRD). The addition of WFC as partial replacement of the cement showed a significant enhancement in the compressive strength for the mortars exposed to normal and elevated temperatures. The compressive strength of the mortar incorporating 20 wt% of WFC and exposed to 700 °C is about 2.5-fold greater than that of the ordinary mortar. Even after exposure to 700 °C, the UPV for the 20 wt% WFC-blended mortar is 30% greater than that for ordinary mortar, indicating the improved structural integrity of the blended mortars. The WFC-blended mortars showed dense and compact microstructure confirming the improvement in the strength of mortars.

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References

  1. Marvila, M.T.; Alexandre, J.; Azevedo, A.R.G.; Zanelato, E.B.; Xavier, G.C.; Monteiro, S.N.: Study on the replacement of the hydrated lime by kaolinitic clay in mortars. Adv. Appl. Ceram. 118(7), 373–380 (2019)

    Article  Google Scholar 

  2. Marvila, M.T.; de Azevedo, A.R.; Alexandre, J.; Colorado, H.; Pereira Antunes, M.L.; Vieira, C.M.: Circular economy in cementitious ceramics: replacement of hydrated lime with a stoichiometric balanced combination of clay and marble waste. Int. J. Appl. Ceram. Technol. 18(1), 192–202 (2021)

    Article  Google Scholar 

  3. Alonso, C.; Fernandez, L.: Dehydration and rehydration processes of cement paste exposed to high temperature environments. J. Mater. Sci. 39(2004), 3015–3024 (2004). https://doi.org/10.1023/B:JMSC.0000025827.65956.18

    Article  Google Scholar 

  4. Burciaga-Díaz, O.; Escalante-García, J.I.: Comparative performance of alkali activated slag/metakaolin cement pastes exposed to high temperatures. Cem. Concr. Compos. 84, 157–166 (2017). https://doi.org/10.1016/j.cemconcomp.2017.09.007

    Article  Google Scholar 

  5. Liu, K.; Cheng, X.; Zhang, C.; Gao, X.; Zhuang, J.; Guo, X.: Evolution of pore structure of oil well cement slurry in suspension–solid transition stage. Constr. Build. Mater. 214, 382–398 (2019). https://doi.org/10.1016/j.conbuildmat.2019.04.075

    Article  Google Scholar 

  6. Morsy, M.; Shoukry, H.; Mokhtar, M.M.; Taha, N.A.; Morsy, M.S.: Systematic investigation into mechanical strength, pore structure and microstructure of high performance concrete incorporating nano-hybrids. IOP Conf.Ser. Mater. Sci. Eng. 956(1), 012001 (2020)

    Article  Google Scholar 

  7. Phan, L.T.; Lawson, J.R.; Davis, F.L.: Effects of elevated temperature exposure on heating characteristics, spalling, and residual properties of high performance concrete. Mater. Struct. 34(2), 83–91 (2001)

    Article  Google Scholar 

  8. Morsy, M.S.; Al-Salloum, Y.A.; Abbas, H.; Alsayed, S.H.: Behavior of blended cement mortars containing nano-metakaolin at elevated temperatures. Constr. Build. Mater. 35, 900–905 (2012)

    Article  Google Scholar 

  9. Cülfik, M.S.; Özturan, T.: Effect of elevated temperatures on the residual mechanical properties of high-performance mortar. Cem. Concr. Res. 32(5), 809–816 (2002)

    Article  Google Scholar 

  10. Nadeem, A.; Memon, S.A.; Lo, T.Y.: The performance of fly ash and metakaolin concrete at elevated temperatures. Constr. Build. Mater. 62, 67–76 (2014)

    Article  Google Scholar 

  11. Liu, K.; Cheng, X.J.; Li, X.; Gao, Y.; Cao, X.; Guo, J.; Zhuang, C. Zhang.: Effects of microstructure and pore water on electrical conductivity of cement slurry during early hydration. Compos. Part B Eng. 177, 1–15 (2019)

    Google Scholar 

  12. Wang, D.; Shi, C.Z.; Wu, J.; Xiao, Z.; Huang, Z. Fang.: A review on ultra-high performance concrete: Part II. Hydration, microstructure and properties. Constr. Build. Mater. 96, 368–377 (2015)

    Article  Google Scholar 

  13. Leonardo, B.; Costa, D.S.; De Souza, G.G.; Cezar, J.; Freitas, D.O.R.; Gomes, P.; Henrique, S.: Santos: silica content in fluence on cement compressive strength in wells subjected to steam injection. J. Pet. Sci. Eng. 158, 626–633 (2017)

    Article  Google Scholar 

  14. Shoukry, H.; Kotkata, M.F.; Abo-El-Enein, S.A.; Morsy, M.S.; Shebl, S.S.: Enhanced physical, mechanical and microstructural properties of lightweight vermiculite cement composites modified with nano metakaolin. Constr. Build. Mater. 112, 276–283 (2017)

    Article  Google Scholar 

  15. Al-Jabri, K.; Shoukry, H.: Influence of nano metakaolin on thermo-physical, mechanical and microstructural properties of high-volume ferrochrome slag mortar. Constr. Build. Mater. 177, 210–221 (2018)

    Article  Google Scholar 

  16. Cheng, X.Q.; Dong, Z.; Li, X.; Guo, W.: Duan,: Influence of potassium titanate whisker on the mechanical properties and microstructure of calcium aluminate cement for in situ combustion. J. Adhes. Sci. Technol. (2017). https://doi.org/10.1080/01694243.2017.1355226

    Article  Google Scholar 

  17. Kirgiz, M.S.: Advancements in mechanical and physical properties for marble powder-cement composites strengthened by nanostructured graphite particles. Mech. Mater. 92, 223–234 (2015). https://doi.org/10.1016/j.mechmat.2015.09.013

    Article  Google Scholar 

  18. Nahm, J. J. W.; Vinegar, H. J.; Karanikas, J. M.; Wyant, R.E.: High temperature wellbore cement slurry (1993)

  19. Sharief, F.A.M.; Moshrif, M.A.: Chronostratigraphy and hydrocarbon prospects of the Sakaka Formation, northern Arabia. J. Petrol. GeoL. 21, 85–102 (1988)

    Google Scholar 

  20. Moshrif, M. A.; Kelling, G.: Stratigraphy and sedimentary history of Upper, Lower and Middle Cretaceous rocks, central Saudi Arabia, Mineral Resources Bull., 28, Directorate General of Mineral Resources, Jeddah, Saudi Arabia, 28 pp (1984)

  21. Abd-El-Aal, A.: Engineering assessment and applications of clays, case study on middle cretaceous (Wasia Formation), Riyadh, KSA. J. Mater. Sci. Eng. 5, 214 (2015)

    Google Scholar 

  22. Gameil, M.; El-Sorogy, A.S.: Gastropods from the campanian–maastrichtian Aruma Formation, Central Saudi Arabia. J. Afr. Earth Sci. 103(2015), 128–139 (2015)

    Article  Google Scholar 

  23. ASTM C150: Standard specification for portland cement. American Society of Testing and Materials (2004)

  24. ASTM C597–16: Standard test method for pulse velocity through concrete. ASTM International, West Conshohocken, PA (2016). www.astm.org

  25. Althoey, F.; Wisner, B.; Kontsos, A.; Farnam, Y.: Cementitious materials exposed to high concentration of sodium chloride solution: formation of a deleterious chemical phase change. Constr. Build. Mater. 167, 543–552 (2018)

    Article  Google Scholar 

  26. Sharma, P.; Khandelwal, M.; Singh, T.: A correlation between Schmidt hammer rebound numbers with impact strength index, slake durability index and P-wave velocity. Int. J. Earth Sci. 100, 189–195 (2011)

    Article  Google Scholar 

  27. ASTM C109/C109M-20b: Standard Test Method for Compressive Strength of Hydraulic Cement Mortars (Using 2-in. or [50 mm] Cube Specimens), ASTM International, West Conshohocken, PA (2020). www.astm.org

  28. Abd El-Aal, A.K.; Salah, M.K.; Khalifa, M.A.: Acoustic and strength characterization of Upper Cretaceous dolostones from the Bahariya Oasis, Western Desert, Egypt: the impact of porosity and diagenesis. J. Petrol. Sci. Eng. 187, 106798 (2020). https://doi.org/10.1016/j.petrol.2019.106798

    Article  Google Scholar 

  29. Rao, D.P.S.; Sravana, D.; Rahim, D.Z.A.; Sekhar, D.T.S.; Aarathi, D.P.: Cracking Behavior of Metakaolin blended high strength concrete in flexure by using crimped steel fibers. J. Civ. Eng. Sci. Int. J. 1, 1–2 (2012)

    Google Scholar 

  30. Rao, D.P.S.; Sravana, D.; Rahim, D.Z.A.; Sekhar, D.T.S.: Durability studies on steel fiber reinforced metakaolin blended concrete. AKGEJC Int. J. Technol. 3(1), 38–43 (2012)

    Google Scholar 

  31. Amaral, L.F.; Delaqua, G.C.G.; Nicolite, M.; Marvila, M.T.; de Azevedo, A.R.; Alexandre, J.; Monteiro, S.N.: Eco-friendly mortars with addition of ornamental stone waste-A mathematical model approach for granulometric optimization. J. Clean Prod. 248, 119283 (2020)

    Article  Google Scholar 

  32. De Azevedo, A.R.G.; Marvila, M.T.; da Silva Barroso, L.; Zanelato, E.B.; Alexandre, J.; de Castro Xavier, G.; Monteiro, S.N.: Effect of granite residue incorporation on the behavior of mortars. Materials 12(9), 1449 (2019)

    Article  Google Scholar 

  33. Althoey, F.; Farnam, Y.: The effect of using supplementary cementitious materials on damage development due to the formation of a chemical phase change in cementitious materials exposed to sodium chloride”. Constr. Build. Mater. 210, 685–695 (2019)

    Article  Google Scholar 

  34. Tsioulou, O.; Lampropoulos, A.; Paschalis, S.: Combined non-destructive testing (NDT) method for the evaluation of the mechanical characteristics of ultra-high performance fibre reinforced concrete (UHPFRC),". Constr. Build. Mater. 131, 66–77 (2017)

    Article  Google Scholar 

  35. Mohammed, B.; Sazmi, N.J.; Abdullahi, M.: Evaluation of rubbercrete based on ultrasonic pulse velocity and rebound hammer tests. Constr. Build. Mater. 25(3), 1388–1397 (2011)

    Article  Google Scholar 

  36. Al-Jabri, K.; Shoukry, H.; Khalil, I.S.; Nasir, S.; Hassan, H.F.: Reuse of waste ferrochrome slag in the production of mortar with improved thermal and mechanical performance. J. Mater. Civ. Eng. 30(8), 04018152 (2018)

    Article  Google Scholar 

  37. Al-Jabri, K.; Shoukry, H.: Use of nano-structured waste materials for improving mechanical, physical and structural properties of cement mortar. Constr. Build. Mater. 73, 636–644 (2014)

    Article  Google Scholar 

Download references

Acknowledgements

This research was conducted in the material and structural laboratory at Najran University and the authors acknowledge the support that has made operation of these facilities possible. Any opinions or discussions provided in this paper are those of the authors. The authors also are indebted to editor in chief of AJSE and the anonymous reviewers for their worthy time and the comments that reconstructed and improved the quality of the study.

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Authors and Affiliations

  1. Civil Engineering Department, Faculty of Engineering, Najran University, Najran, Kingdom of Saudi Arabia

    Fadi Althoey, Ahmed K. Abd El-Aal & Ibrahim Hakeem

  2. Geology Department, Faculty of Science, Al-Azhar University, Assiut Branch, Cairo, Egypt

    Ahmed K. Abd El-Aal

  3. Housing and Building National Research Center (HBRC), Building Physics Institute (BPI), Cairo, Egypt

    Hamada Shoukry

Authors
  1. Fadi Althoey
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  2. Ahmed K. Abd El-Aal
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  3. Hamada Shoukry
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  4. Ibrahim Hakeem
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Correspondence to Ahmed K. Abd El-Aal.

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Althoey, F., El-Aal, A.K.A., Shoukry, H. et al. Performance of Cement Mortars Containing Clay Exposed to High Temperature. Arab J Sci Eng 47, 591–599 (2022). https://doi.org/10.1007/s13369-021-05583-x

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  • DOI: https://doi.org/10.1007/s13369-021-05583-x

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