Graphitization cracks in Ck45 steel clips of turbofans
Introduction
The fasteners, clamps and clips are important in different industries. Since these parts work as a connecting component, their performance is critical [1], [2], [3], [4].
Some studies have been done on graphitization of different steels, Ye Jin Kim and et al. [5] investigated the effect of heat treatment temperature and primary grain size on the mechanical properties and graphitization. Zhang and Han [6] surveyed graphitization of free- cutting steels and Guseva et al. [7] investigated the methods of graphitized steels obtaining when there is a need for both steel and gray cast iron properties.
Carbon steels are used due to the variety of mechanical properties provided when suitable heat treatment is used [8]. During the steel production, it is essential that raw material has enough quality, cleanliness, and pass the quality control checks [9].
A small company provided seven coils of DIN Ck45 for production of turbofan clips. When company used new coils of DIN Ck45 faced with the failure problem. It is noticeable that the failure was just observed in one coil out of the seven coils. The failure was observed during the forming of turbofan clips in related stamping die. These products are formed in progressive dies during 8 stages. The progressive die design of the turbofan clips can be seen in Fig. 1. In the 1th, 2nd and 8th stages cracks form in the parts.
As it is shown in Fig. 2, the turbofan clip is a component that holds electromotor. Assembling was done using impact force and the failure of the new specimen was observed during the impact assembling. In order to improve the formability and proper hardness, the microstructure of raw materials was selected to contain alpha ferrite + spheroidized cementite instead of ferrite + pearlite. The products were passed martempering process before assembling. The process of martempering heat treatment was consisted of austenitizing of parts at 860 °C for 15 min and tempering at 330 °C for 1 h with 420 HV. The furnace used in this study was shaker heart type made by SIB (Italian brand).
The production process needed for raw materials was hot rolling until the plate reaches to adequate thickness. Then cold rolling was done for final dimension and finally spheroidizing annealing (or soft annealing) was done using inter critical annealing at 850 °C and 700 °C for total 80 h at hydrogen atmosphere in order to recrystallization and spheroidizing, and to reduce hardness and increase the formability of coils. There was a brittle failure problem in one coil. There are some hypothesizes for this failure and this paper tries to present the reasons of the failure.
Section snippets
Chemical analysis
Chemical analysis of DIN Ck45 (EN 1.1191) coils were provided to determine the probable effects of differences in chemical elements based on ASTM E415-17 as mentioned in Table 1.
Mechanical tests
Hardness and tensile tests were used to measure the mechanical strength of coils. The tensile test was done based on ISO 6892-1 (2019) standard and the test was done using GOTECH tensile machine with displacement rate of 0.0075 mm/s based on dimensions in Fig. 3.
Micro hardness experiments were done using Future Tech
Results
Chemical analysis of DIN Ck45 coils in Table 2 does not show a considerable difference between elements of proper and failed materials. Although these variations are limited, they can play minor role in graphitization process. The effect of different elements on graphitization has been surveyed in many researches [10], [11], [12], Woo et al. investigated Boron in graphitization and mentioned that small addition of Si, Al, Ni, Cr and Mn can differ the graphitization. Woo et al. investigated the
Discussion
Many reasons cause failure in steels such as strain age embrittlement, temper embrittlement, sigma phase embrittlement and graphitization. This graphitization is often reported in carbon steels held at temperatures over 425 °C [14]. Generally, graphitization phenomenon explained as a formation of graphite (free form of carbon) in iron or steel matrix [15], [16]. In terms of thermodynamic, cementite is a meta-stable intermetallic phase from combination of iron and carbon elements which can be
Conclusions
- 1.
It seems that spheroidize annealing was not done properly and the temperature and time was at the range in which graphitization occurs, and one of the coils does not meet the required formability and it is actually like gray cast iron. Unfortunately, due to stability of graphite phase, it was not possible to repair these coils and became disposal. The interesting point is that the coil properties were at acceptable ranges of DIN 17,222 standard for cold rolled steel strip. The chemical analysis
Declaration of Competing Interest
The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.
Acknowledgement
This research was supported by Foulad Fam Company in Iran and the authors would like to thank Mr. Ali Goorani (Factory manager) because of his supportive colaboration in providing necessary facilities to do this research and his helpful ideas.
References (24)
- et al.
Graphitization behavior of medium-carbon high-silicon steel and its dependence on temperature and grain size
J. Mater. Sci. Eng. A
(2020) - et al.
Effects of B and Ti addition and heat treatment temperature on graphitization behavior of Fe-0.55 C-2.3 Si steel
J. Mater. Res. Tech.
(2020) - et al.
The influence of different heat treatment cycles on controlled surface graphitization in CK45 steel
J. Alloy. Comp.
(2010) - et al.
The influence of annealing temperature on the graphitisation of CK 45 Steel
J. Alloy. Comp.
(2009) Failure analysis in engineering applications
(2014)- et al.
Metallurgical failure analysis
McGraw-Hill, Inc. (USA)
(1993) - et al.
An investigation of the cause of failure in a spring hose clamp
J. Fail. Anal. Prevent.
(2020) - et al.
Motorcycle hose clamp failure analysis
J. Fail. Anal. Prevent.
(2017) - et al.
A study of graphitization of free-cutting steel
J. Met. Sci. Heat. Treat.
(2019) - et al.
Methods of graphitized steels obtaining
J. Phys: Conf. Seri.
(2019)
Graphitization behaviors of creep-ruptured 0.3% carbon steel at 673 to 773˚K
J. ISIJ. Inter.
State of the art in evaluation and control of steel cleanliness
J. ISIJ. Inter.
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