Graphitization cracks in Ck45 steel clips of turbofans

https://doi.org/10.1016/j.engfailanal.2021.105402Get rights and content

Highlights

  • In this research the failure of a DIN Ck45-steelclips of turbofans during the forming was studied.

  • The failure was originated from a problem with raw material.

  • The problem was related to the slow rate of heating beneath of 850 °C.

  • It seems that spheroidize annealing was not done properly and the temperature and time was at the range in which graphitization occurs.

Abstract

In this research the failure of a DIN Ck45-steelclip of a turbofan during the forming process was studied. As the failure was brittle and the forming was done properly, the failure was originated from a problem with raw material. The material and properties like chemical compound, hardness and tensile strength were at the proper ranges. The cold rolled steel passed the heat treatment process like spheroidize annealing and martempering prior using as clips. The problem was related to the slow rate of heating beneath of 850 °C and incomplete microstructure modifying prior to spheroidizing annealing which causes the graphitization in the raw material, and brittle failure during the forming process of parts.

Introduction

The fasteners, clamps and clips are important in different industries. Since these parts work as a connecting component, their performance is critical [1], [2], [3], [4].

Some studies have been done on graphitization of different steels, Ye Jin Kim and et al. [5] investigated the effect of heat treatment temperature and primary grain size on the mechanical properties and graphitization. Zhang and Han [6] surveyed graphitization of free- cutting steels and Guseva et al. [7] investigated the methods of graphitized steels obtaining when there is a need for both steel and gray cast iron properties.

Carbon steels are used due to the variety of mechanical properties provided when suitable heat treatment is used [8]. During the steel production, it is essential that raw material has enough quality, cleanliness, and pass the quality control checks [9].

A small company provided seven coils of DIN Ck45 for production of turbofan clips. When company used new coils of DIN Ck45 faced with the failure problem. It is noticeable that the failure was just observed in one coil out of the seven coils. The failure was observed during the forming of turbofan clips in related stamping die. These products are formed in progressive dies during 8 stages. The progressive die design of the turbofan clips can be seen in Fig. 1. In the 1th, 2nd and 8th stages cracks form in the parts.

As it is shown in Fig. 2, the turbofan clip is a component that holds electromotor. Assembling was done using impact force and the failure of the new specimen was observed during the impact assembling. In order to improve the formability and proper hardness, the microstructure of raw materials was selected to contain alpha ferrite + spheroidized cementite instead of ferrite + pearlite. The products were passed martempering process before assembling. The process of martempering heat treatment was consisted of austenitizing of parts at 860 °C for 15 min and tempering at 330 °C for 1 h with 420 HV. The furnace used in this study was shaker heart type made by SIB (Italian brand).

The production process needed for raw materials was hot rolling until the plate reaches to adequate thickness. Then cold rolling was done for final dimension and finally spheroidizing annealing (or soft annealing) was done using inter critical annealing at 850 °C and 700 °C for total 80 h at hydrogen atmosphere in order to recrystallization and spheroidizing, and to reduce hardness and increase the formability of coils. There was a brittle failure problem in one coil. There are some hypothesizes for this failure and this paper tries to present the reasons of the failure.

Section snippets

Chemical analysis

Chemical analysis of DIN Ck45 (EN 1.1191) coils were provided to determine the probable effects of differences in chemical elements based on ASTM E415-17 as mentioned in Table 1.

Mechanical tests

Hardness and tensile tests were used to measure the mechanical strength of coils. The tensile test was done based on ISO 6892-1 (2019) standard and the test was done using GOTECH tensile machine with displacement rate of 0.0075 mm/s based on dimensions in Fig. 3.

Micro hardness experiments were done using Future Tech

Results

Chemical analysis of DIN Ck45 coils in Table 2 does not show a considerable difference between elements of proper and failed materials. Although these variations are limited, they can play minor role in graphitization process. The effect of different elements on graphitization has been surveyed in many researches [10], [11], [12], Woo et al. investigated Boron in graphitization and mentioned that small addition of Si, Al, Ni, Cr and Mn can differ the graphitization. Woo et al. investigated the

Discussion

Many reasons cause failure in steels such as strain age embrittlement, temper embrittlement, sigma phase embrittlement and graphitization. This graphitization is often reported in carbon steels held at temperatures over 425 °C [14]. Generally, graphitization phenomenon explained as a formation of graphite (free form of carbon) in iron or steel matrix [15], [16]. In terms of thermodynamic, cementite is a meta-stable intermetallic phase from combination of iron and carbon elements which can be

Conclusions

  • 1.

    It seems that spheroidize annealing was not done properly and the temperature and time was at the range in which graphitization occurs, and one of the coils does not meet the required formability and it is actually like gray cast iron. Unfortunately, due to stability of graphite phase, it was not possible to repair these coils and became disposal. The interesting point is that the coil properties were at acceptable ranges of DIN 17,222 standard for cold rolled steel strip. The chemical analysis

Declaration of Competing Interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Acknowledgement

This research was supported by Foulad Fam Company in Iran and the authors would like to thank Mr. Ali Goorani (Factory manager) because of his supportive colaboration in providing necessary facilities to do this research and his helpful ideas.

References (24)

  • T. Hatakeyama et al.

    Graphitization behaviors of creep-ruptured 0.3% carbon steel at 673 to 773˚K

    J. ISIJ. Inter.

    (2020)
  • L. Zhang et al.

    State of the art in evaluation and control of steel cleanliness

    J. ISIJ. Inter.

    (2003)
  • Cited by (5)

    • Failure analysis of CK45 steel crankshaft in light truck diesel engine

      2023, Engineering Failure Analysis
      Citation Excerpt :

      Unfortunately, due to the lack of chromium in CK45 steel, it often suffers from corrosion and rust. Applications of this material are recommended for crankshafts, shafts, axles, and industrial rollers under high temperatures, fatigue loads, and dynamic loads [1,2]. The main part of any internal combustion engine is its crankshaft, whose job is to convert the linear motion of the piston into rotational motion.

    • Failure Analysis of a 17-4PH Stainless Steel Part in an Exhaust Fastener

      2021, Journal of Failure Analysis and Prevention
    View full text