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Electrochemical Detection of Ascorbic acid in Orange on Iron(III) Oxide Nanoparticles Modified Screen Printed Carbon Electrode

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Abstract

This study reports the electrochemical detection of ascorbic acid (AA) at screen printed carbon electrode (SPCE) modified with iron(III) oxide nanoparticle. Iron(III) nanoparticle was synthesized from Callistemon viminalis leaf extract (CV-Fe3O4NP). SPCE/CV-Fe3O4NP electrode showed faster electron transport in terms of the current response to AA oxidation compare to bare SPCE, which is due to the presence of CV-Fe3O4NP. The dynamic range for the detection of AA was from 10 to 100 μM. Limit of detection for AA on modified SPCE/CV-Fe3O4NP electrode was 15.7 μM which compared favorably with other electrodes investigated. The selectivity of the modified SPCE/CV-Fe3O4NP electrode was also determined. The designed sensor showed good selectivity to AA in the presence of interfering specie DA of same concentration (0.1 mM). Real sample analysis was carried out to establish the practical feasibility of the developed sensor (SPCE/CV-Fe3O4NP).

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Acknowledgements

Authors acknowledged the assistance of MASIIM of North-West University, NRF-Thutuka grant and the Higher Degree of North-West University, Mafikeng Campus are also acknowledged.

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  1. Department of Chemistry, Faculty of Natural and Agricultural Sciences, North-West University (Mafikeng Campus), Private Bag X2046, Mmabatho, 2735, South Africa

    Gloria E. Uwaya & Omolola E. Fayemi

  2. Material Science Innovation and Modelling (MaSIM) Research Focus Area, Faculty of Natural and Agricultural Sciences, North-West University (Mafikeng Campus), Private Bag X2046, Mmabatho, 2735, South Africa

    Gloria E. Uwaya & Omolola E. Fayemi

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  1. Gloria E. Uwaya
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OEF conceptualized and designed the work and was part of the manuscript write-up. GEU carried out the experiments, interpreted some of the results and were also involved in the manuscript preparation. All the authors reviewed the manuscript and have agreed to its publication.

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Correspondence to Omolola E. Fayemi.

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Uwaya, G.E., Fayemi, O.E. Electrochemical Detection of Ascorbic acid in Orange on Iron(III) Oxide Nanoparticles Modified Screen Printed Carbon Electrode. J Clust Sci 33, 1035–1043 (2022). https://doi.org/10.1007/s10876-021-02030-7

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