Abstract
In the present survey, a nitrogen-doped amorphous carbon nanocomposite has been prepared simply and eco-friendly from heating an acidic solution of sorbitol and urea. It was used as an efficient sorbent in dispersive solid phase extraction for the extraction of some pesticides (chlorpyrifos, diniconazole, clodinafop–propargyl, oxadiazon, fenpropathrin and penconazole) from fruit juice samples. The method was followed by a dispersive liquid–liquid microextraction procedure for more preconcentration of the analytes. The extracted analytes were determined by gas chromatography–flame ionization detection. Under optimized experimental conditions, relative standard deviations were in the ranges of 3–5% and 5–7% for intra-day (n = 6) and inter-day (n = 4) precisions, respectively, at a concentration of 10 μg L−1 for each analyte. The limits of detection and quantification were in the ranges of 0.89–1.3 and 3.0–4.3 μg L−1, respectively. The linear ranges were achieved in the range of 3.0–2000 μg L−1. Also, enrichment factors and extraction recoveries were obtained in the ranges of 380–455 and 76–91%, respectively. Finally, the developed approach was performed to determine the studied pesticide residues in various fruit juices including pomegranate, sour cherry, grape, orange and apple.
Similar content being viewed by others
Change history
24 August 2023
A Correction to this paper has been published: https://doi.org/10.1007/s13738-023-02871-1
Abbreviations
- ACNC :
-
Amorphous carbon nanocomposite
- DLLME :
-
Dispersive liquid–liquid microextraction
- DSPE :
-
Dispersive solid phase extraction
- EF :
-
Enrichment factor
- ER :
-
Extraction recovery
- FID :
-
Flame ionization detector
- GC :
-
Gas chromatography
- LOD :
-
Limit of detection
- LOQ :
-
Limit of quantification
- SPE :
-
Solid phase extraction
References
R.C. Gilden, K. Huffling, B. Sattler, J. Obstet. Gynecol. Neonatal. Nurs. 376, 103 (2010)
P.C. Jepson, K. Murray, O. Bach, M.A. Bonilla, L. Neumeister, Lancet Planet. Health 4, e56 (2020)
A.K. Harding, G.P. Daston, G.R. Boyd, G.W. Lucier, S.H. Safe, J. Stewart, D.E. Tillitt, G.V. Der Kraak, Environ. Health Perspect. 114, 1276 (2006)
M.A. Farajzadeh, A. Mohebbi, B. Feriduni, Anal. Methods 8, 5676 (2016)
M. Abbaspour, M.A. Farajzadeh, S.M. Sorouraddin, A. Mohebbi, Anal. Methods 11, 4022 (2019)
A. Diuzheva, H. Dejmková, J. Fischer, V. Andruch, Microchem. J. 150, 104071 (2019)
M.A. Farajzadeh, H. Sohrabi, A. Mohebbi, Food Anal. Methods 12, 534 (2019)
G. Dugo, G.D. Bella, L.L. Torre, M. Saitta, Food Control 16, 435 (2005)
M.A. Farajzadeh, A. Mohebbi, V. Tofigh Gharamaleki, M. Abbaspour, S.M. Sorouraddin, New J. Chem. 43, 12453 (2019)
M.A. Farajzadeh, A. Mohebbi, A. Pazhohan, M. Nemati, MR Afshar Mogaddam. Trends Anal. Chem. 110, 8 (2019)
T. Hyötyläinen, Anal. Bioanal. Chem. 394, 743 (2009)
M. Nasiri, H. Ahmadzadeh, A. Amiri, Trends Anal. Chem. 123, 115772 (2020)
B. Buszewski, M. Szultka, Crit. Rev. Anal. Chem. 42, 198 (2012)
J. Plotka-Wasylka, N. Szczepanska, M. Guardia, J. Namieśnik, Trends Anal. Chem. 73, 19 (2015)
M. Anastassiades, S.J. Lehotay, D. Stajnbaher, F.J. Schenck, J. AOAC Int. 86, 412 (2003)
F. Khalilian, S. Amiri Hanzaki, M. Yousefi, J. Sep. Sci. 38, 975 (2015)
M.Á. González-Curbelo, A.V. Herrera-Herrera, J. Hernández-Borges, M.Á. Rodríguez-Delgado, J. Sep. Sci. 36, 556 (2013)
Q. Wu, C. Wang, Z. Liu, C. Wu, X. Zeng, J. Wen, Z. Wang, J. Chromatogr. A 1216, 5504 (2009)
Y. Zhang, H. Xu, Food Anal. Methods 7, 189 (2014)
M. Rezaee, Y. Assadi, M.R. Milani Hosseini, E. Aghaee, F. Ahmadi, S. Berijani, J. Chromatogr. A 1, 160 (2006)
C. Almeida, J.O. Fernandes, S.C. Cunha, Food Control 25, 380 (2012)
Y. Han, X. Jia, X. Liu, T. Duan, H. Chen, J. Sep. Sci. 34, 1047 (2011)
A. Sarafraz-Yazdi, H. Assadi, W.A. Wan Ibrahim, Ind. Eng. Chem. Res. 51, 3101 (2012)
L.M. Ravelo-Pérez, J. Hernández-Borges, M.Á. Rodríguez-Delgado, J. Chromatogr. A 1211, 33 (2008)
Y.L. Gao, P. Sun, Acta Chromatogr. 30, 141 (2018)
H. Bagheri, S. Asgari, H. Piri-Moghadam, Chromatographia 77, 723 (2014)
A. Navalon, A. Prieto, L. Araujo, J.L. Vılchez, J. Chromatogr. A 946, 239 (2002)
B. Maddah, A. Sabouri, M. Hasanzadeh, J. Polym. Environ. 25, 770 (2017)
S. Bodur, C. Özlü, B. Tışlı, M. Fırat, D.S. Chormey, S. Bakırdere, Environ. Monit. Assess. 192, 253 (2020)
M.A. Farajzadeh, M. Sattari Dabbagh, A. Yadeghari, J. Sep. Sci. 40, 2253 (2017)
M. Pirsaheb, N. Fattahi, M. Shamsipur, Food Control 34, 378 (2013)
Acknowledgements
The authors thank the Research Council of University of Tabriz for financial support.
Funding
Mir Ali Farajzadeh has received research grants from University of Tabriz.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
The authors declare that they have no conflict of interest.
Ethical approval
This article does not contain any studies with human or animals.
Rights and permissions
Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
About this article
Cite this article
Farajzadeh, M.A., Davaran, M., Mohebbi, A. et al. Dispersive solid phase extraction based on simply prepared nitrogen-doped amorphous carbon nanocomposite combined with dispersive liquid–liquid microextraction: application in the extraction of some pesticides from fruit juices. J IRAN CHEM SOC 18, 2151–2164 (2021). https://doi.org/10.1007/s13738-021-02180-5
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s13738-021-02180-5