Issue 4, 2021
From the journal:

New Journal of Chemistry

Catalytic synthesis of benzannelated macrocyclic di- and triperoxides based on phenols

Nataliya N. Makhmudiyarova, ORCID logo *a   Irina R. Ishmukhametova,a   Kamil R. Shangaraev,a   Lilya U. Dzhemileva,*a   Vladimir A. D'yakonov,a   Askhat G. Ibragimova  and  Usein M. Dzhemileva  

* Corresponding authors

a Institute of Petrochemistry and Catalysis, Russian Academy of Sciences, 141 prospekt Oktyabrya, 450075 Ufa, Russian Federation
E-mail: natali-mnn@mail.ru, dzhemilev@mail.ru

Abstract

An efficient method for the synthesis of benzannelated macrocyclic di- and triperoxides by cyclocondensation of phenol, catechol, resorcinol or hydroquinone with bis-hydroperoxides and formaldehyde in the presence of lanthanide catalysts has been developed. Additionally, by using flow cytometry, it has been shown for the first time in this work that thus-synthesized macrocyclic di- and triperoxides are efficient apoptosis inducers in the tumor cultures Jurkat, K562 and U937 and in fibroblasts.

Graphical abstract: Catalytic synthesis of benzannelated macrocyclic di- and triperoxides based on phenols

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Article information

DOI
https://doi.org/10.1039/D0NJ05511E
Article type
Paper
Submitted
11 Nov 2020
Accepted
27 Dec 2020
First published
18 Jan 2021

New J. Chem., 2021,45, 2069-2077

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Catalytic synthesis of benzannelated macrocyclic di- and triperoxides based on phenols

N. N. Makhmudiyarova, I. R. Ishmukhametova, K. R. Shangaraev, L. U. Dzhemileva, V. A. D'yakonov, A. G. Ibragimov and U. M. Dzhemilev, New J. Chem., 2021, 45, 2069 DOI: 10.1039/D0NJ05511E

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