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The Peculiarities of the Sample Preparation of Bottom Sediments for ICP-MS Elemental Analysis

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—Two methods of sample preparation (microwave assisted acid digestion and sintering with sodium bicarbonate) of materials with complex compositions, including organic components for ICP-MS elemental analysis, were tested. The samples used included terrigenous clay (SDO-1), volcanic-terrigenous silt (SDO-2), calcareous silt (SDO-3), ferromanganese nodules (SDO-5), Baikal silt (BIL-1), and a complex sample of Baikal sediments (BIL-2). The most effective sample preparation routines for the studied rocks are proposed.

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Correspondence to Ya. V. Bychkova, D.P. Starodymova, K. V. Shaikhutdinova, D. R. Dyagileva, M. A. Semernin, E. M. Dekunova, I. Yu. Nikolaeva or A. Yu. Bychkov.

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This study was supported by the Russian Foundation for Basic Research (project no. 18-05-00818).

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Translated by M. Nickolsky

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Bychkova, Y.V., Starodymova, D., Shaikhutdinova, K.V. et al. The Peculiarities of the Sample Preparation of Bottom Sediments for ICP-MS Elemental Analysis. Moscow Univ. Geol. Bull. 75, 496–505 (2020). https://doi.org/10.3103/S0145875220050038

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  • DOI: https://doi.org/10.3103/S0145875220050038

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