Abstaract
—Two methods of sample preparation (microwave assisted acid digestion and sintering with sodium bicarbonate) of materials with complex compositions, including organic components for ICP-MS elemental analysis, were tested. The samples used included terrigenous clay (SDO-1), volcanic-terrigenous silt (SDO-2), calcareous silt (SDO-3), ferromanganese nodules (SDO-5), Baikal silt (BIL-1), and a complex sample of Baikal sediments (BIL-2). The most effective sample preparation routines for the studied rocks are proposed.
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REFERENCES
Arnautov, N.V., Standartnye obraztsy khimicheskogo sostava prirodnykh mineral’nykh veshchestv. Metodicheskie rekomendatsii. 2-e izd. (Standard Samples of Chemical Composition of Natural Mineral Substances. Methodological Recommendations (2nd ed.)), Novosibirsk, 1990.
Berkovits, L.A. and Lukashin, V.N., Three marine sediment reference samples: SDO-1, SDO-2 and SDO-3, Geostand. Newl., 1984, vol. 8, no. 1, pp. 51–56.
Berkovits, L.A., Obol’yaninova, V.G., and Baturin, G.N., Composition of standard reference samples of Fe–Mn nodules and bottom sediments, Okeanologiya, 1990, vol. 30, no. 3, pp. 455–463.
Bychkova, Ya.V., Sinitsyn, M.Yu., Petrenko, D.B., et al., Method peculiarities of multielemental analysis of rocks with inductively-coupled plasma mass spectrometry, Moscow Univ. Geol. Bull., 2017, vol. 72, no. 1, pp. 56–62.
Bychkova, Ya.V., Nikolaeva, I.Yu., Ermina, O.C., et al., Methodical peculiarities of preparation of solid geological samples for multi-element analysis by ICP-MS, Moscow Univ. Geol. Bull., 2018, no. 5, pp. 53–59.
Dauvalter, V.A., Geoekologiya donnykh otlozhenii ozer (Geoecology of Bottom Sediments in Lakes), Murmansk: Murmansk. Gos. Tekhn. Univ., 2012.
Dubinin, A.V., Induction-coupled plasma mass-spectrometry: Detection of rare elements in standard samples from oceanic sediments, Geokhimiya, 1993, no. 11, pp. 1605–1619.
Dubinin, A.V., Geokhimiya redkozemel’nykh elementov v okeane (Geochemistry of Rare Earth Elements in Ocean), Moscow: Nauka, 2006.
GOST (State Standard) 5180-84: Soils. Laboratory Methods for Determination of Physical characteristics, Moscow: Standartinform, 2016.
Katalog standartnykh obraztsov sostava prirodnykh i tekhnogennykh sred (Catalog of Reference Standard Samples from Natural and Man-Made Environments), Irkutsk, 2013.
Lavrushin, V.Yu., Subsurface fluids of the Greater Caucasus and its frame, in Tr. GIN, vyp. 599 (Trans. Geol. Inst. Vol. 599), Moscow: GEOS, 2012.
Lisitsyn, A.P., Protsessy okeanskoi sedimentatsii (Processes of the Oceanic Sedimentation), Moscow: Nauka, 1978.
Perel’man, A.I. and Kasimov, N.S., Geokhimiya landshafta (Landscape Geochemistry), Moscow: Astreya-2000, 1999.
Stein, R., Chapter four proxies used for palaeoenvironmental reconstructions in the Arctic Ocean, Develop. Marin. Geol., 2008, vol. 2, pp. 133–243.
Strekopytov, S.V. and Dubinin, A.V., Determination of Mo, W, and Th contents in standard samples SDO (oceanic sediments and ores) by ICP-MS technique, Oceanology, 1996, vol. 36, no. 6, pp. 816–818.
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This study was supported by the Russian Foundation for Basic Research (project no. 18-05-00818).
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Translated by M. Nickolsky
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Bychkova, Y.V., Starodymova, D., Shaikhutdinova, K.V. et al. The Peculiarities of the Sample Preparation of Bottom Sediments for ICP-MS Elemental Analysis. Moscow Univ. Geol. Bull. 75, 496–505 (2020). https://doi.org/10.3103/S0145875220050038
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DOI: https://doi.org/10.3103/S0145875220050038