Abstract
The development of inhomogeneity in the microstructure, texture, and mechanical property in hot-rolled (API) 5L X70 pipeline steel after rough and finish thermomechanical control processing has been investigated by experimental measurements. Our investigations revealed that the rough rolling stage produced mostly large and coarse ferrite grains across the thickness, while the finish rolling stage led to a rather refined small-grained microstructure. EBSD investigations confirmed that after the rough rolling stage, recovered and deformed grains dominated the quarter and mid-thickness compared to the surface. Investigation of the finish rolled steel showed that in comparison with the quarter and mid-thickness sections of the plate, the surface section mostly consists of deformed grains. The texture components obtained from x-ray measurement showed that after rough and finish processing stages, the {001} <100>, {110} <112>, {123} <634>, {112} <111>, and {001} <110> components were observed to be present. However, inhomogeneity of texture was observed at different depths of the rolled steel, such that in comparison with the surface, volume fractions of texture and intensities of the desired γ-fiber texture were seen to be highest at the mid- and quarter-thickness sections after both rolling stages. The room-temperature tensile stress–strain curves showed that the highest yield strength was observed for samples obtained from the near-surface section, while samples obtained from the mid-thickness section showed the highest elongation during tensile deformation. Overall, the final stage processing was observed to refine the final microstructure of the steel, thus improving the strength of the steel.
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M.Y. Huh, H.C. Kim, J.J. Park, and O. Engler, Evolution of Through-Thickness Texture Gradients in Various Steel Sheets, Met. Mater. Int., 1999, 5(5), p 437–443
E.J. Pickering and M. Holland, Detection of Macrosegregation in a Large Metallic Specimen Using XRF, Ironmak. Steelmak., 2014, 41(7), p 493–499
R.E. Hook, Physical Asymmetry of the Crystallographic Texture of an Interstitial-Free Sheet Steel, Metall. Mater. Trans. A, 1993, 2009(24), p 2009–2019
H. Mizukami, K. Hayashi, M. Numata, and A. Yamanaka, Prediction of Solid–Liquid Interfacial Energy of Steel During Solidification and Control of Dendrite Arm Spacing, ISIJ Int., 2011, 97(9), p 457–466
Y.B. Park, D.N. Lee, and G. Gottstein, Effect of Hot Rolling Condition on the Development of Textures in Ultra Low Carbon Steel, J. Mater. Process. Technol., 1994, 45(1–4), p 471–476
K.T. Kim, S.G. Ko, and J.M. Han, Effects of Microstructural Inhomogeneity on HIC Susceptibility Ipc2014-33341 2014, p 1–8
A.I. Fedosseev and D. Raabe, Application of the Method of Superposition of Harmonic Currents for the Simulation of Inhomogeneous Deformation During Hot Rolling of FeCr, Scr. Metall. Mater., 1994, 30(1), p 1–6
C.C. Tasan, J.P.M. Hoefnagels, and M.G.D. Geers, Microstructural Banding Effects Clarified Through Micrographic Digital Image Correlation, Scr. Mater., 2010, 62, p 835–838
A.A. Korda, Y. Mutoh, Y. Miyashita, T. Sadasue, and S.L. Mannan, In Situ Observation of Fatigue Crack Retardation in Banded Ferrite-Pearlite Microstructure Due to Crack Branching, Scr. Mater., 2006, 54, p 1835–1840
Y.B. Park, D.N. Lee, and G. Gottstein, Development of Texture Inhomogeneity During Hot Rolling in Interstitial Free Steel, Acta Mater., 1996, 44(8), p 3421–3427
Y.W. Kim, J.H. Kim, S.G. Hong, and C.S. Lee, Effects of Rolling Temperature on the Microstructure and Mechanical Properties of Ti-Mo Microalloyed Hot-Rolled High Strength Steel, Mater. Sci. Eng. A, 2014, 605, p 244–252
Y. Liu, F. Zhu, Y. Li, and G. Wang, Effect of TMCP Parameters on the Microstructure and Properties of an Nb-Ti Microalloyed Steel, ISIJ Int., 2005, 45(6), p 851–857
X.J. Shen, S. Tang, Y.J. Wu, X.L. Yang, J. Chen, Z.Y. Liu, R.D.K. Misra, and G.D. Wang, Evolution of Microstructure and Crystallographic Texture of Microalloyed Steel During Warm Rolling in Dual Phase Region and Their Influence on Mechanical Properties, Mater. Sci. Eng. A, 2017, 685, p 194–204
S. Vervynckt, K. Verbeken, B. Lopez, and J.J. Jonas, Modern HSLA Steels and Role of Non-Recrystallisation Temperature, Int. Mater. Rev., 2012, 57(4), p 187–207
V. Carretero Olalla, V. Bliznuk, N. Sanchez, P. Thibaux, L.A.I. Kestens, and R.H. Petrov, Analysis of the Strengthening Mechanisms in Pipeline Steels as a Function of the Hot Rolling Parameters, Mater. Sci. Eng. A, 2014, 604, p 46–56. https://doi.org/10.1016/j.msea.2014.02.066
S. Nafisi, M.A. Arafin, L. Collins, and J. Szpunar, Texture and Mechanical Properties of API X100 Steel Manufactured Under Various Thermomechanical Cycles, Mater. Sci. Eng. A, 2012, 531, p 2–11
M.R. Toroghinejad, A.O. Humphreys, D. Liu, F. Ashrafizadeh, A. Najafizadeh, and J.J. Jonas, Effect of Rolling Temperature on the Deformation and Recrystallization Textures of Warm-Rolled Steels, Metall. Mater. Trans. A., 2003, 34(5), p 1163–1174
A. Haldar and R.K. Ray, Microstructural and Textural Development in an Extra Low Carbon Steel During Warm Rolling, Mater. Sci. Eng. A, 2005, 391(1–2), p 402–407
R.K. Ray and A. Haldar, Texture Development in Extra Low Carbon (ELC) and Interstitial Free (IF) Steels During Warm Rolling, Mater. Manuf. Process., 2002, 17(5), p 715–729
D. Raabe and K. Lücke, Texture and Microstructure of Hot Rolled Steel, Scr. Metall. Mater., 1992, 26(8), p 1221–1226
D. Raabe, Overview on Basic Types of Hot Rolling Textures of Steels, Steel Res. Int., 2003, 74(5), p 327–337
P. Siahpour, R. Miresmaeili, and A. Sabour Rouhaghdam, Temperature Effect of Hot Rolling Process on Microstructure, Strength and Fracture Toughness of X65 Pipeline Steel, Trans. Indian Inst. Met., 2018, 71(6), p 1531–1541
M.A. Mohtadi-Bonab, M. Eskandari, and J.A. Szpunar, Texture, Local Misorientation, Grain Boundary and Recrystallization Fraction in Pipeline Steels Related to Hydrogen Induced Cracking, Mater. Sci. Eng. A, 2014, 620, p 97–106
V. Venegas, F. Caleyo, L.E. Vázquez, T. Baudin, and J.M. Hallen, On the Influence of Crystallographic Texture on Pitting Corrosion in Pipeline Steels, Int. J. Electrochem. Sci., 2015, 10(4), p 3539–3552
V. Venegas, F. Caleyo, J.M. Hallen, T. Baudin, and R. Penelle, Role of Crystallographic Texture in Hydrogen-Induced Cracking of Low Carbon Steels for Sour Service Piping, Metall. Mater. Trans. A Phys. Metall. Mater. Sci., 2007, 38(5), p 1022–1031
V. Venegas, F. Caleyo, J.L. González, T. Baudin, J.M. Hallen, and R. Penelle, EBSD Study of Hydrogen-Induced Cracking in API-5L-X46 Pipeline Steel, Scr. Mater., 2005, 52(2), p 147–152
M.A. Arafin and J.A. Szpunar, A New Understanding of Intergranular Stress Corrosion Cracking Resistance of Pipeline Steel Through Grain Boundary Character and Crystallographic Texture Studies, Corros. Sci., 2009, 51(1), p 119–128
R.K. Ray and J.J. Jonas, Transformation Textures in Steels, Int. Met. Rev., 1990, 35(1), p 1–36
R.K. Ray, J.J. Jonas, P. Butron, and J. Savoie, Transformation Texture in Steels, ISIJ Int., 1994, 34(12), p 927–942
P.K.C. Venkatsurya, R.D.K. Misra, M.D. Mulholland, M. Manohar, and J.E. Hartmann, Effect of Microstructure on the Mechanical Properties and Texture in High Strength 560 MPa Linepipe Steels, Mater. Sci. Eng. A, 2013, 575, p 6–14
J.J. Jonas (Ed.), Transformation Textures Associated with Steel Processing, Springer, 2009, p 3–17
J.-Y. Kang, D.-I. Kim, and H.-C. Lee, Texture Development in Low Carbon Sheet Steels for Automotive Application, Springer, 2009, p 85–101
P. Juntunen, P. Karjalainen, D. Raabe, G. Bolle, and T. Kopio, Optimizing Continuous Annealing of Interstitial-Free Steels for Improving Deep Drawability, Metall. Mater. Trans. A Phys. Metall. Mater. Sci, 2001, 32(8), p 1989–1995
D. Raabe, Texture of Strip Cast and Hot Rolled Ferritic and Austenitic Stainless Steel, Mater. Sci. Technol., 1995, 11(6), p 461–468
D. Raabe, Texture and Microstructure Evolution During Cold Rolling of a Strip Cast and of a Hot Rolled Austenitic Stainless Steel, Acta Mater., 1997, 45(3), p 1137–1151
J.I. Omale, E.G. Ohaeri, A.A. Tiamiyu, M. Eskandari, K.M. Mostafijur, and J.A. Szpunar, Microstructure, Texture Evolution and Mechanical Properties of X70 Pipeline Steel After Different Thermomechanical Treatments, Mater. Sci. Eng. A, 2017, 703(July), p 477–485
J.I. Omale, E.G. Ohaeri, J.A. Szpunar, M. Arafin, and F. Fateh, Microstructure and Texture Evolution in Warm Rolled API 5L X70 Pipeline Steel for Sour Service Application, Mater. Charact., 2019, 147, p 453–463.
W.B. Hutchinson, L. Ryde, and P.S. Bate, Transformation Textures in Steels, Mater. Sci. Forum, 2005, 495–497, p 1141–1150
Y. He, S. Godet, and J.J. Jonas, Representation of Misorientations in Rodrigues-Frank Space: Application to the Bain, Kurdjumov-Sachs, Nishiyama-Wassermann and Pitsch Orientation Relationships in the Gibeon Meteorite, Acta Mater., 2005, 53(4), p 1179–1190
M.N. Ei-ichi Furubayashi and H. Miyaji, Simple Model of Predicting the Transformation Textures in Thermomechanically Processed Steels, Trans. Iron Steel Inst. Jpn, 1987, 27(6), p 513–519
E.O. Hall, The Deformation and Aging of Mild Steel, Proc. Phys. Soc. Sect. B, 1951, 64(9), p 747
N. Hansen, Hall–Petch Relation and Boundary Strengthening, Scr. Mater., 2004, 51(8 SPEC. ISS.), p 801–806
R. Shukla, S.K. Ghosh, D. Chakrabarti, and S. Chatterjee, Microstructure, Texture, Property Relationship in Thermo-Mechanically Processed Ultra-Low Carbon Microalloyed Steel for Pipeline Application, Mater. Sci. Eng. A, 2013, 587, p 201–208
Acknowledgments
The authors are grateful to the Natural Sciences and Engineering Research Council of Canada (NSERC strategic Grant: 470033). We also thank Evraz Inc. in Regina and CANMET, Natural Resources Canada, Hamilton, for the supply of steel samples and conducting all the thermomechanical treatments.
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Omale, J.I., Ohaeri, E.G., Mostafijur, K.M. et al. Through-Thickness Inhomogeneity of Texture, Microstructure, and Mechanical Properties After Rough and Finish Rolling Treatments in Hot-Rolled API 5L X70 Pipeline Steel. J. of Materi Eng and Perform 29, 8130–8144 (2020). https://doi.org/10.1007/s11665-020-05280-0
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DOI: https://doi.org/10.1007/s11665-020-05280-0